acetic acid 2-(4-benzyloxy-phenyl)-1-(2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-ethyl ester

Base Information

• Chemical Name: acetic acid 2-(4-benzyloxy-phenyl)-1-(2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-ethyl ester
• CAS No.: 387333-74-6
• Molecular Formula: C₃₁H₃₆N₂O₆
• Molecular Weight: 532.637

Synonyms:acetic acid 2-(4-benzyloxy-phenyl)-1-(2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-ethyl ester

Chemical Property of acetic acid 2-(4-benzyloxy-phenyl)-1-(2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-ethyl ester

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Technology Process of acetic acid 2-(4-benzyloxy-phenyl)-1-(2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-ethyl ester

There total 1 articles about acetic acid 2-(4-benzyloxy-phenyl)-1-(2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

lead(IV) tetraacetate (546-67-8) + (S)-3-(4-Benzyloxy-phenyl)-2-((S)-2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-propionic acid → acetic acid 2-(4-benzyloxy-phenyl)-1-(2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-ethyl ester (387333-74-6)

Guidance literature:

With pyridine; copper diacetate; In tetrahydrofuran; at 0 - 25 ℃;

DOI:10.1021/jo0158027

Reference yield: 45.0%

acetic acid 2-(4-benzyloxy-phenyl)-1-(2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-ethyl ester (387333-74-6) → {(S)-1-[(Z)-2-(4-Benzyloxy-phenyl)-vinylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester

Guidance literature:

With lithium perchlorate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 25 ℃;

DOI:10.1021/jo0158027

Reference yield:

acetic acid 2-(4-benzyloxy-phenyl)-1-(2-tert-butoxycarbonylamino-3-phenyl-propionylamino)-ethyl ester (387333-74-6) → {(S)-1-[(Z)-2-(4-Benzyloxy-phenyl)-vinylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester + {(S)-1-[(E)-2-(4-Benzyloxy-phenyl)-vinylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 25 ℃; Title compound not separated from byproducts.;

DOI:10.1021/jo0158027

upstream raw materials:

lead(IV) tetraacetate

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