C₂₉H₄₆O₇

Base Information

Chemical Name:C₂₉H₄₆O₇
CAS No.:1448230-69-0
Molecular Formula:C₂₉H₄₆O₇
Molecular Weight:506.68
Hs Code.:

C<sub>29</sub>H<sub>46</sub>O<sub>7</sub>

Synonyms:C₂₉H₄₆O₇

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Chemical Property of C₂₉H₄₆O₇

Chemical Property:

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Technology Process of C₂₉H₄₆O₇

There total 8 articles about C₂₉H₄₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448230-68-9
C₂₉H₄₆O₇

: 1448230-69-0
C₂₉H₄₆O₇

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; at 0 - 20 ℃; for 7.5h;
DOI:10.1021/ol4017518

Reference yield:

: 1448230-65-6
C₃₂H₆₇IO₄Si₂

: 1448230-69-0
C₂₉H₄₆O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

1.2: 0.33 h / 20 °C

1.3: 13 h / 50 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

3.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

With tetrabutyl ammonium fluoride; tert.-butyl lithium; pyridinium p-toluenesulfonate; 9-methoxy-9-BBN; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; pentane;
DOI:10.1021/ol4017518

Reference yield:

: C₂₂H₃₄O₄

: 1448230-69-0
C₂₉H₄₆O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III); osmium(VIII) oxide; methanesulfonamide; potassium carbonate / water; tert-butyl alcohol / 23 h / 0 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.17 h / 20 °C / pH 7

4.1: triethylamine; dmap / dichloromethane / 25 h / 0 - 20 °C

5.1: sodium iodide / acetone / 18 h / 50 °C

6.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

6.2: 0.33 h / 20 °C

6.3: 13 h / 50 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

8.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

With 2,6-dimethylpyridine; dmap; osmium(VIII) oxide; methanesulfonamide; tetrabutyl ammonium fluoride; tert.-butyl lithium; pyridinium p-toluenesulfonate; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; 9-methoxy-9-BBN; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; acetone; tert-butyl alcohol; pentane; 1.1: |Sharpless Dihydroxylation;
DOI:10.1021/ol4017518