[((η3-C3H5)Pd)2(μ,κ2:κ2-C(Ph2P=NSiMe3)2)]

Base Information

• Chemical Name: [((η3-C3H5)Pd)2(μ,κ2:κ2-C(Ph2P=NSiMe3)2)]
• CAS No.: 1202896-30-7
• Molecular Formula: C₃₇H₄₈N₂P₂Pd₂Si₂
• Molecular Weight: 851.76
• Mol file: 1202896-30-7.mol

Synonyms:[((η3-C3H5)Pd)2(μ,κ2:κ2-C(Ph2P=NSiMe3)2)]

Chemical Property of [((η3-C3H5)Pd)2(μ,κ2:κ2-C(Ph2P=NSiMe3)2)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [((η3-C3H5)Pd)2(μ,κ2:κ2-C(Ph2P=NSiMe3)2)]

There total 1 articles about [((η3-C3H5)Pd)2(μ,κ2:κ2-C(Ph2P=NSiMe3)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

bis(η3-allyl-μ-chloropalladium(II)) + [bis(diphenyltrimethylsilyliminophosphorano)methanediide)Li2]2 → [((η3-C3H5)Pd)2(μ,κ2:κ2-C(Ph2P=NSiMe3)2)] (1202896-30-7)

Guidance literature:

In benzene; byproducts: LiCl; under Ar or N2; to a benzene soln. of Li-contg. compd. (0.15 mmol) was added Pd-contg. compd. (0.30 mmol) as a solid in a single portion at roomtemp.; stirring at room temp. for 2-3 h; the filtered soln. was evapd. on a dynamic vac. line; the residue was dissolved in ether; LiCl was removed by centrifugation; the soln. was evapd. under vac.; elem. anal.;

DOI:10.1021/om900571k

Reference yield:

[((η3-C3H5)Pd)2(μ,κ2:κ2-C(Ph2P=NSiMe3)2)] (1202896-30-7) → palladium (7440-05-3)

Guidance literature:

In not given; under Ar or N2; by heating at 115°C in C6H6 or C7H8;

DOI:10.1021/om900571k

Downstream raw materials:

palladium