[2-Chloro-3-(4-methoxy-phenyl)-1-(4-nitro-phenyl)-3-oxo-propyl]-thiocarbamic acid S-methyl ester

Base Information

Chemical Name:[2-Chloro-3-(4-methoxy-phenyl)-1-(4-nitro-phenyl)-3-oxo-propyl]-thiocarbamic acid S-methyl ester
CAS No.:91358-50-8
Molecular Formula:C₁₈H₁₇ClN₂O₅S
Molecular Weight:408.862
Hs Code.:

Synonyms:[2-Chloro-3-(4-methoxy-phenyl)-1-(4-nitro-phenyl)-3-oxo-propyl]-thiocarbamic acid S-methyl ester

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Chemical Property of [2-Chloro-3-(4-methoxy-phenyl)-1-(4-nitro-phenyl)-3-oxo-propyl]-thiocarbamic acid S-methyl ester

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Technology Process of [2-Chloro-3-(4-methoxy-phenyl)-1-(4-nitro-phenyl)-3-oxo-propyl]-thiocarbamic acid S-methyl ester

There total 2 articles about [2-Chloro-3-(4-methoxy-phenyl)-1-(4-nitro-phenyl)-3-oxo-propyl]-thiocarbamic acid S-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 91358-44-0
(4-Methoxy-phenyl)-[(4S,5S)-2-methylsulfanyl-4-(4-nitro-phenyl)-4,5-dihydro-oxazol-5-yl]-methanone

: 91358-50-8
[2-Chloro-3-(4-methoxy-phenyl)-1-(4-nitro-phenyl)-3-oxo-propyl]-thiocarbamic acid S-methyl ester

Guidance literature:: With hydrogenchloride; In dichloromethane; for 0.0833333h; Heating;

Reference yield:

: 27547-03-1,32157-65-6
(4-Methoxy-phenyl)-[(2S,3R)-3-(4-nitro-phenyl)-oxiranyl]-methanone

: 91358-50-8
[2-Chloro-3-(4-methoxy-phenyl)-1-(4-nitro-phenyl)-3-oxo-propyl]-thiocarbamic acid S-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / 1) Aluminum chloride, 2) aq. KHCO₃ / CH₂Cl₂ / 20 - 25 °C

2: 96 percent / Dry hydrogen chloride / CH₂Cl₂ / 0.08 h / Heating

With hydrogenchloride; aluminium trichloride; potassium hydrogencarbonate; In dichloromethane;