N-Pyridin-3-yl-cyclohexanecarboximidothioic acid pyridin-2-yl ester

Base Information

Chemical Name:N-Pyridin-3-yl-cyclohexanecarboximidothioic acid pyridin-2-yl ester
CAS No.:119541-42-3
Molecular Formula:C₁₇H₁₉N₃S
Molecular Weight:297.424
Hs Code.:

Synonyms:N-Pyridin-3-yl-cyclohexanecarboximidothioic acid pyridin-2-yl ester

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Chemical Property of N-Pyridin-3-yl-cyclohexanecarboximidothioic acid pyridin-2-yl ester

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Technology Process of N-Pyridin-3-yl-cyclohexanecarboximidothioic acid pyridin-2-yl ester

There total 2 articles about N-Pyridin-3-yl-cyclohexanecarboximidothioic acid pyridin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 105398-69-4
Cyclohexanecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester

: 85526-38-1
3-pyridyl isocyanide

: 119541-42-3
N-Pyridin-3-yl-cyclohexanecarboximidothioic acid pyridin-2-yl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at -15 ℃; for 0.416667h; Irradiation;
DOI:10.1016/S0040-4020(01)85980-9

Reference yield:

: 462-08-8
pyridin-3-ylamine

: 119541-42-3
N-Pyridin-3-yl-cyclohexanecarboximidothioic acid pyridin-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / 50percent aq. NaOH / n-Bu₄NHSO₄ / CH₂Cl₂; CHCl₃ / 12 h

2: 70 percent / trifluoroacetic acid / CH₂Cl₂ / 0.42 h / -15 °C / Irradiation

With sodium hydroxide; trifluoroacetic acid; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; chloroform;
DOI:10.1016/S0040-4020(01)85980-9