[bis(3,5-dimethylpyrazole)bis(μ-3,5-dimethylpyrazolate)(2,6-pyridine dicarboxylate)dipalladium(II)]

Base Information

Chemical Name:[bis(3,5-dimethylpyrazole)bis(μ-3,5-dimethylpyrazolate)(2,6-pyridine dicarboxylate)dipalladium(II)]
CAS No.:917366-53-1
Molecular Formula:C₂₇H₃₃N₉O₄Pd₂
Molecular Weight:760.457
Hs Code.:

Synonyms:[bis(3,5-dimethylpyrazole)bis(μ-3,5-dimethylpyrazolate)(2,6-pyridine dicarboxylate)dipalladium(II)]

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Chemical Property of [bis(3,5-dimethylpyrazole)bis(μ-3,5-dimethylpyrazolate)(2,6-pyridine dicarboxylate)dipalladium(II)]

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Technology Process of [bis(3,5-dimethylpyrazole)bis(μ-3,5-dimethylpyrazolate)(2,6-pyridine dicarboxylate)dipalladium(II)]

There total 1 articles about [bis(3,5-dimethylpyrazole)bis(μ-3,5-dimethylpyrazolate)(2,6-pyridine dicarboxylate)dipalladium(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 67-51-6
3,5-dimethyl-1H-pyrazole

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 4220-17-1
pyridine-2,6-dicarboxylic acid, monosodium salt

: 917366-53-1
[bis(3,5-dimethylpyrazole)bis(μ-3,5-dimethylpyrazolate)(2,6-pyridine dicarboxylate)dipalladium(II)]

Guidance literature:: In methanol; water; PdCl2(CH3CN)2 dissolved in MeOH; to this added methanolic soln. of 3,5-dimethylpyrazole; mixture stirred for 10 min at room temp.; filtered off to remove any suspended material; aq. NaH2,6-dipic added to filtrate; soln. warmed at 50 °C for 30 min; soln. cooled to room temp; crystals obtained after 7 days; elem. anal.;
DOI:10.1016/j.poly.2006.05.030