C₄₃H₆₇N₅O₈S

Base Information

• Chemical Name: C₄₃H₆₇N₅O₈S
• CAS No.: 1009093-21-3
• Molecular Formula: C₄₃H₆₇N₅O₈S
• Molecular Weight: 814.1
• Mol file: 1009093-21-3.mol

Synonyms:C₄₃H₆₇N₅O₈S

Chemical Property of C₄₃H₆₇N₅O₈S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₃H₆₇N₅O₈S

There total 16 articles about C₄₃H₆₇N₅O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

C9H22N2O2S (1009093-26-8) + C34H47N3O7 (1009091-78-4) → C43H67N5O8S (1009093-21-3)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

C8H10INO2 (874347-50-9) → C43H67N5O8S (1009093-21-3)

Guidance literature:

Multi-step reaction with 7 steps

1.1: benzene / Heating / reflux

2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

2.2: 2 h

3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

4.1: trimethylaluminum / hexane; dichloromethane / 0.25 h

4.2: 20 °C

4.3: 2 h

5.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 36 h / 60 °C

6.1: sodium cyanoborohydride; acetic acid / methanol; water / 2 h / 20 °C

7.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 1 h / 20 °C

With titanium(IV) isopropylate; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; acetic acid; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; toluene; benzene;

Reference yield:

C11H12INO4 (1009091-77-3) → C43H67N5O8S (1009093-21-3)

Guidance literature:

Multi-step reaction with 6 steps

1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

1.2: 2 h

2.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

3.1: trimethylaluminum / hexane; dichloromethane / 0.25 h

3.2: 20 °C

3.3: 2 h

4.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 36 h / 60 °C

5.1: sodium cyanoborohydride; acetic acid / methanol; water / 2 h / 20 °C

6.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 1 h / 20 °C

With titanium(IV) isopropylate; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; acetic acid; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; toluene;

upstream raw materials:

C₉H₂₂N₂O₂S

C₃₄H₄₇N₃O₇

C₈H₁₀INO₂

C₁₁H₁₂INO₄