2-(2H-1,2,3-benzotriazol-2-yl)-5-tert-butyl-4-hydroxybenzenecarboxaldehyde

Base Information

Chemical Name:2-(2H-1,2,3-benzotriazol-2-yl)-5-tert-butyl-4-hydroxybenzenecarboxaldehyde
CAS No.:861395-96-2
Molecular Formula:C₁₇H₁₇N₃O₂
Molecular Weight:295.341
Hs Code.:

Synonyms:2-(2H-1,2,3-benzotriazol-2-yl)-5-tert-butyl-4-hydroxybenzenecarboxaldehyde

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Chemical Property of 2-(2H-1,2,3-benzotriazol-2-yl)-5-tert-butyl-4-hydroxybenzenecarboxaldehyde

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Technology Process of 2-(2H-1,2,3-benzotriazol-2-yl)-5-tert-butyl-4-hydroxybenzenecarboxaldehyde

There total 6 articles about 2-(2H-1,2,3-benzotriazol-2-yl)-5-tert-butyl-4-hydroxybenzenecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 861395-94-0
2-(2H-1,2,3-benzotriazol-2-yl)-6-tert-butyl-4-dibromomethylphenyl acetate

: 861395-96-2
2-(2H-1,2,3-benzotriazol-2-yl)-5-tert-butyl-4-hydroxybenzenecarboxaldehyde

Guidance literature:: With sodium acetate; In methanol; water; for 6h; Heating;
DOI:10.3987/COM-04-10304

Reference yield:

: 2-(tert-butyl)-4-methyl-6-[(E)-2-(2-nitrophenyl)diazenyl]benzenol

: 861395-96-2
2-(2H-1,2,3-benzotriazol-2-yl)-5-tert-butyl-4-hydroxybenzenecarboxaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: 81 percent / zinc; sodium hydroxide / ethanol / 5 h / 100 °C

2.1: sulfuric acid / 1 h / 20 °C

2.2: 93 percent / 1 h / Heating

3.1: 66 percent / N-bromosuccinimide (NBS); α,α'-bis-azo-isobutyronitrile / CCl4 / 24 h / Heating

4.1: 88 percent / sodium acetate trihydrate / methanol; H₂O / 6 h / Heating

With sodium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sulfuric acid; sodium acetate; zinc; In methanol; tetrachloromethane; ethanol; water;
DOI:10.3987/COM-04-10304

Reference yield:

: 861395-93-9
2-(2H-1,2,3-benzotriazol-2-yl)-6-(tert-butyl)-4-methylphenyl acetate

: 861395-96-2
2-(2H-1,2,3-benzotriazol-2-yl)-5-tert-butyl-4-hydroxybenzenecarboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / N-bromosuccinimide (NBS); α,α'-bis-azo-isobutyronitrile / CCl4 / 24 h / Heating

2: 88 percent / sodium acetate trihydrate / methanol; H₂O / 6 h / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium acetate; In methanol; tetrachloromethane; water;
DOI:10.3987/COM-04-10304