Technology Process of (6-thioacetylmethyl)ubiquinone
There total 7 articles about (6-thioacetylmethyl)ubiquinone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium cerium (IV) nitrate;
In
water; acetonitrile;
at 0 - 20 ℃;
for 0.833333h;
DOI:10.1021/ja204014s
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / ethanol; water / 0 - 20 °C
2: titanium tetrachloride / dichloromethane / 0 - 20 °C
3: potassium borohydride / ethanol / 0.5 h / 0 °C
4: phosphorus tribromide / tetrahydrofuran / 0.5 h / 0 °C
5: tetrahydrofuran / 4 h / Reflux; Inert atmosphere
6: ammonium cerium (IV) nitrate / water; acetonitrile / 0.83 h / 0 - 20 °C
With
ammonium cerium (IV) nitrate; potassium borohydride; phosphorus tribromide; titanium tetrachloride; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ja204014s
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium borohydride / methanol / 0.5 h / 0 °C
2: sodium hydroxide / ethanol; water / 0 - 20 °C
3: titanium tetrachloride / dichloromethane / 0 - 20 °C
4: potassium borohydride / ethanol / 0.5 h / 0 °C
5: phosphorus tribromide / tetrahydrofuran / 0.5 h / 0 °C
6: tetrahydrofuran / 4 h / Reflux; Inert atmosphere
7: ammonium cerium (IV) nitrate / water; acetonitrile / 0.83 h / 0 - 20 °C
With
ammonium cerium (IV) nitrate; potassium borohydride; phosphorus tribromide; titanium tetrachloride; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ja204014s
