C₃₃H₄₂O₆Si

Base Information

Chemical Name:C₃₃H₄₂O₆Si
CAS No.:1610935-80-2
Molecular Formula:C₃₃H₄₂O₆Si
Molecular Weight:562.778
Hs Code.:

C<sub>33</sub>H<sub>42</sub>O<sub>6</sub>Si

Synonyms:C₃₃H₄₂O₆Si

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Chemical Property of C₃₃H₄₂O₆Si

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Technology Process of C₃₃H₄₂O₆Si

There total 14 articles about C₃₃H₄₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₄₂O₆Si

: 1610935-80-2
C₃₃H₄₂O₆Si

: C₃₃H₄₂O₆Si

Guidance literature:: With sodium methylate; In methanol; at 0 ℃; for 3h; Overall yield = 81 %; Overall yield = 41.1 mg;
DOI:10.1021/ol501301w

Reference yield:

: 237057-62-4
(E)-1-tert-Butyldimethylsilyloxy-6-hydroxy-hex-3-ene

: 1610935-80-2
C₃₃H₄₂O₆Si

: C₃₃H₄₂O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 0.17 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C / Inert atmosphere

2.2: 2 h / 0 - 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C / Inert atmosphere

3.2: 4 h / 0 - 20 °C

4.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 24 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 0.67 h / 0 °C

6.1: 24 h / 20 °C

7.1: AD-mix β; methanesulfonamide / tert-butyl alcohol; water / 12 h / 0 °C

8.1: sodium methylate / methanol / 3 h / 0 °C

With 1H-imidazole; n-butyllithium; methanesulfonamide; AD-mix β; iodine; sodium methylate; Dess-Martin periodane; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; methanol; hexane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol501301w

Reference yield:

: 1610935-53-9
(E)-tert-butyl((6-iodohex-3-en-1-yl)oxy)dimethylsilane

: 1610935-80-2
C₃₃H₄₂O₆Si

: C₃₃H₄₂O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C / Inert atmosphere

2.2: 4 h / 0 - 20 °C

3.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 24 h / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 0.67 h / 0 °C

5.1: 24 h / 20 °C

6.1: AD-mix β; methanesulfonamide / tert-butyl alcohol; water / 12 h / 0 °C

7.1: sodium methylate / methanol / 3 h / 0 °C

With n-butyllithium; methanesulfonamide; AD-mix β; sodium methylate; Dess-Martin periodane; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol501301w