Sodium; (Z)-7-[(1S,2R,3R,4R)-3-(4-hydroxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoate

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Chemical Name:Sodium; (Z)-7-[(1S,2R,3R,4R)-3-(4-hydroxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoate
CAS No.:115267-09-9
Molecular Formula:C₂₀H₂₆NO₅S*Na
Molecular Weight:415.486
Hs Code.:

Synonyms:Sodium; (Z)-7-[(1S,2R,3R,4R)-3-(4-hydroxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoate

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Chemical Property of Sodium; (Z)-7-[(1S,2R,3R,4R)-3-(4-hydroxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoate

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Technology Process of Sodium; (Z)-7-[(1S,2R,3R,4R)-3-(4-hydroxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoate

There total 2 articles about Sodium; (Z)-7-[(1S,2R,3R,4R)-3-(4-hydroxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 115206-16-1
(Z)-7-[(1S,2R,3R,4R)-3-(4-Acetoxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoic acid

: 115267-09-9
Sodium; (Z)-7-[(1S,2R,3R,4R)-3-(4-hydroxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoate

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1021/jm00117a028

Reference yield:

: 115206-12-7
(Z)-7-[(1S,2R,3R,4R)-3-(4-Acetoxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoic acid methyl ester

: 115267-09-9
Sodium; (Z)-7-[(1S,2R,3R,4R)-3-(4-hydroxy-benzenesulfonylamino)-bicyclo[2.2.1]hept-2-yl]-hept-5-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1 N KOH / methanol / 6 h / 23 °C

2: 87 percent / sodium methoxide / methanol

With potassium hydroxide; sodium methylate; In methanol;
DOI:10.1021/jm00117a028