C₁₄H₁₁N₅O₃

Base Information

Chemical Name:C₁₄H₁₁N₅O₃
CAS No.:1338084-40-4
Molecular Formula:C₁₄H₁₁N₅O₃
Molecular Weight:297.273
Hs Code.:

C<sub>14</sub>H<sub>11</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₁₄H₁₁N₅O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₁N₅O₃

Chemical Property:

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Technology Process of C₁₄H₁₁N₅O₃

There total 4 articles about C₁₄H₁₁N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1338083-83-2
C₁₆H₁₅N₅O₃

: 1338084-40-4
C₁₄H₁₁N₅O₃

Guidance literature:: With ethanol; sodium hydroxide; at 20 ℃; Reflux;
DOI:10.1016/j.bmcl.2011.08.022

Reference yield:

: 120445-48-9,3030-95-3
4-methylbenzaldehyde semicarbazone

: 1338084-40-4
C₁₄H₁₁N₅O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine; sodium acetate / acetic acid / 0.5 h / 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 5 - 20 °C / Inert atmosphere

2.2: 5 °C / Inert atmosphere

3.1: ethanol; sodium hydroxide / 20 °C / Reflux

With ethanol; bromine; sodium acetate; sodium hydride; sodium hydroxide; In tetrahydrofuran; acetic acid; mineral oil;
DOI:10.1016/j.bmcl.2011.08.022

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 1338084-40-4
C₁₄H₁₁N₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate / water / 20 °C

2.1: bromine; sodium acetate / acetic acid / 0.5 h / 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 5 - 20 °C / Inert atmosphere

3.2: 5 °C / Inert atmosphere

4.1: ethanol; sodium hydroxide / 20 °C / Reflux

With ethanol; bromine; sodium acetate; sodium hydride; sodium hydroxide; In tetrahydrofuran; water; acetic acid; mineral oil;
DOI:10.1016/j.bmcl.2011.08.022