5-Phenethyl-4-hydroxy-1,2,5-thiadiazolidin-3-one 1,1-dioxide sodium salt

Base Information

Chemical Name:5-Phenethyl-4-hydroxy-1,2,5-thiadiazolidin-3-one 1,1-dioxide sodium salt
CAS No.:130670-00-7
Molecular Formula:C₁₀H₁₁N₂O₄S*Na
Molecular Weight:278.264
Hs Code.:

Synonyms:5-Phenethyl-4-hydroxy-1,2,5-thiadiazolidin-3-one 1,1-dioxide sodium salt

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Chemical Property of 5-Phenethyl-4-hydroxy-1,2,5-thiadiazolidin-3-one 1,1-dioxide sodium salt

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Technology Process of 5-Phenethyl-4-hydroxy-1,2,5-thiadiazolidin-3-one 1,1-dioxide sodium salt

There total 2 articles about 5-Phenethyl-4-hydroxy-1,2,5-thiadiazolidin-3-one 1,1-dioxide sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 130669-99-7
2-Phenethyl-1,2,5-thiadiazolidine-3,4-dione 1,1-dioxide sodium salt

: 130670-00-7
5-Phenethyl-4-hydroxy-1,2,5-thiadiazolidin-3-one 1,1-dioxide sodium salt

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jo00312a013

Reference yield:

: 4455-09-8
2-phenylethyl tosylate

: 130670-00-7
5-Phenethyl-4-hydroxy-1,2,5-thiadiazolidin-3-one 1,1-dioxide sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / dimethylsulfoxide / 72 h / Ambient temperature

2: 62 percent / NaBH₄ / tetrahydrofuran / Ambient temperature

With sodium tetrahydroborate; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/jo00312a013