N_α-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid

Base Information

Chemical Name:N_α-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid
CAS No.:109273-47-4
Molecular Formula:C₂₆H₃₀N₄O₄S*ClH
Molecular Weight:531.076
Hs Code.:

N<sub>α</sub>-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid

Synonyms:N_α-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid

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Chemical Property of N_α-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid

Chemical Property:

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Technology Process of N_α-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid

There total 5 articles about N_α-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 108460-09-9
N_α-(2-Naphthylsulfonylglycyl)-4-nitro-phenylalaninpiperidid

: 109273-47-4
N_α-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid

Guidance literature:: With hydrogenchloride; ammonia; hydrogen; nickel; In methanol;

Reference yield:

: 110-89-4
piperidine

: 109273-47-4
N_α-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-ethyl morpholine, chlorocarbon isobutylester / 1.) acetic ester, 25 min; 2.) 4 h, room temperature

2: 23 percent / 1.) NH₃/hydrogen; 2.) HCl / 1.) Raney-Ni / methanol

With N-ethylmorpholine;; hydrogenchloride; chlorocarbon isobutylester; ammonia; hydrogen; nickel; In methanol;

Reference yield:

: 66693-69-4,147065-06-3
2-amino-3-(4-nitrophenyl)propionic acid hydrochloride

: 109273-47-4
N_α-(2-Naphthylsulfonylglycyl)-4-amino-phenylalaninpiperididhydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / aqu. NaOH / ethyl acetate / 5 h

2: 1.) N-ethyl morpholine, chlorocarbon isobutylester / 1.) acetic ester, 25 min; 2.) 4 h, room temperature

3: 23 percent / 1.) NH₃/hydrogen; 2.) HCl / 1.) Raney-Ni / methanol

With N-ethylmorpholine;; hydrogenchloride; sodium hydroxide; chlorocarbon isobutylester; ammonia; hydrogen; nickel; In methanol; ethyl acetate;