2,5-dimethylbenzylsuccinic acid

Base Information

Chemical Name:2,5-dimethylbenzylsuccinic acid
CAS No.:31318-44-2
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

Synonyms:2,5-dimethylbenzylsuccinic acid

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Chemical Property of 2,5-dimethylbenzylsuccinic acid

Chemical Property:

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Technology Process of 2,5-dimethylbenzylsuccinic acid

There total 6 articles about 2,5-dimethylbenzylsuccinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5779-94-2
2,5-dimethylbenzaldehyde

: 106-65-0
Dimethyl succinate

: 31318-44-2
2,5-dimethylbenzylsuccinic acid

Guidance literature:: 2,5-dimethylbenzaldehyde; Dimethyl succinate; With sodium hydride; In toluene; Reflux;

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 24h;
DOI:10.1080/00304948.2020.1780887

Reference yield:

: 106-42-3
para-xylene

: 31318-44-2
2,5-dimethylbenzylsuccinic acid

Guidance literature:: Multi-step reaction with 4 steps

1: (i) ZnCl₂, (ii) HCl

2: (i) NaOEt, EtOH, (ii) /BRN= 2206277/

3: NaOEt / ethanol

4: aq. NaOH

With sodium hydroxide; sodium ethanolate; In ethanol;
DOI:10.1246/bcsj.45.2871

Reference yield:

: 38303-49-0
Aethyl-aceto-2,5-dimethylbenzylacetat

: 31318-44-2
2,5-dimethylbenzylsuccinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: NaOEt / ethanol

2: aq. NaOH

With sodium hydroxide; sodium ethanolate; In ethanol;
DOI:10.1246/bcsj.45.2871