(3-Benzyloxycarbonylamino-propyl)-[4-(tert-butyl-diphenyl-silanyloxy)-butyl]-carbamic acid benzyl ester

Base Information

• Chemical Name: (3-Benzyloxycarbonylamino-propyl)-[4-(tert-butyl-diphenyl-silanyloxy)-butyl]-carbamic acid benzyl ester
• CAS No.: 204061-15-4
• Molecular Formula: C₃₉H₄₈N₂O₅Si
• Molecular Weight: 652.906

Synonyms:(3-Benzyloxycarbonylamino-propyl)-[4-(tert-butyl-diphenyl-silanyloxy)-butyl]-carbamic acid benzyl ester

Chemical Property of (3-Benzyloxycarbonylamino-propyl)-[4-(tert-butyl-diphenyl-silanyloxy)-butyl]-carbamic acid benzyl ester

Chemical Property:

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Technology Process of (3-Benzyloxycarbonylamino-propyl)-[4-(tert-butyl-diphenyl-silanyloxy)-butyl]-carbamic acid benzyl ester

There total 4 articles about (3-Benzyloxycarbonylamino-propyl)-[4-(tert-butyl-diphenyl-silanyloxy)-butyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(benzyloxycarbonyl)-3-amino-1-propyl methanesulfonate (174626-34-7) → (3-Benzyloxycarbonylamino-propyl)-[4-(tert-butyl-diphenyl-silanyloxy)-butyl]-carbamic acid benzyl ester (204061-15-4)

Guidance literature:

Multi-step reaction with 3 steps

1: K₂CO₃ / CHCl₃

2: Et₃N, DMAP / CH₂Cl₂

3: Et₃N / CH₂Cl₂ / Ambient temperature

With dmap; potassium carbonate; triethylamine; In dichloromethane; chloroform;

DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

Reference yield:

benzyl N-(3-bromopropyl)carbamate (39945-54-5) → (3-Benzyloxycarbonylamino-propyl)-[4-(tert-butyl-diphenyl-silanyloxy)-butyl]-carbamic acid benzyl ester (204061-15-4)

Guidance literature:

Multi-step reaction with 3 steps

1: K₂CO₃ / CHCl₃

2: Et₃N, DMAP / CH₂Cl₂

3: Et₃N / CH₂Cl₂ / Ambient temperature

With dmap; potassium carbonate; triethylamine; In dichloromethane; chloroform;

DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

Reference yield:

N1-(benzyloxycarbonyl)-1-amino-4-azaoctanol-8 → (3-Benzyloxycarbonylamino-propyl)-[4-(tert-butyl-diphenyl-silanyloxy)-butyl]-carbamic acid benzyl ester (204061-15-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N, DMAP / CH₂Cl₂

2: Et₃N / CH₂Cl₂ / Ambient temperature

With dmap; triethylamine; In dichloromethane;

DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

upstream raw materials:

benzyl chloroformate

benzyl N-(3-bromopropyl)carbamate

N-(benzyloxycarbonyl)-3-amino-1-propyl methanesulfonate

Downstream raw materials:

N¹-cholesteryloxycarbonyl-4,9,14-triaza-N^4,14,17-tri(phenylmethoxycarbonyl)heptadecane-1,17-diamine

C₅₄H₈₂N₄O₆

C₅₃H₈₀N₄O₆

{3-[(4-Azido-butyl)-benzyloxycarbonyl-amino]-propyl}-carbamic acid benzyl ester

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