5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE

Base Information

Chemical Name:5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE
CAS No.:338399-40-9
Molecular Formula:C₁₅H₁₆ClNO₂
Molecular Weight:277.751
Hs Code.:2922390090
Mol file:338399-40-9.mol

Synonyms:5-(4-chloro-phenyl)-2-dimethylaminomethylene-cyclohexane-1,3-dione

Suppliers and Price of 5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE 95.00%
1MG
$ 658.53

American Custom Chemicals Corporation
5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE 95.00%
10MG
$ 692.49

American Custom Chemicals Corporation
5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE 95.00%
5MG
$ 697.51

Total 2 raw suppliers

Chemical Property of 5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE

There total 3 articles about 5-(4-CHLOROPHENYL)-2-[(DIMETHYLAMINO)METHYLENE]-1,3-CYCLOHEXANEDIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 27463-38-3
5-(4-chlorophenyl)cyclohexane-1,3-dione

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 338399-40-9
5-(4-chloro-phenyl)-2-dimethylaminomethylene-cyclohexane-1,3-dione

Guidance literature:: In chloroform; at 20 ℃; for 0.5h;

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 338399-40-9
5-(4-chloro-phenyl)-2-dimethylaminomethylene-cyclohexane-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water / 24 h / 0 - 20 °C

2.1: sodium methylate / methanol / 1 h / Reflux

2.2: 2 h / Reflux

3.1: chloroform / 0.5 h / 20 °C

With sodium methylate; sodium hydroxide; In methanol; chloroform; water;

Reference yield:

: 30626-03-0
(3E)-4-(4-chlorophenyl)-3-buten-2-one

: 338399-40-9
5-(4-chloro-phenyl)-2-dimethylaminomethylene-cyclohexane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 1 h / Reflux

1.2: 2 h / Reflux

2.1: chloroform / 0.5 h / 20 °C

With sodium methylate; In methanol; chloroform;