(Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane

Base Information

Chemical Name:(Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane
CAS No.:1384256-34-1
Molecular Formula:C₁₇H₂₀Cl₂N₂O₂
Molecular Weight:355.264
Hs Code.:

Synonyms:(Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane

Suppliers and Price of (Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane

There total 3 articles about (Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89123-81-9
2,2-dichlorobutanoyl chloride

: 1384256-33-0
1-acetyl-2-benzyl-1,4,5,6-tetrahydropyrimidine

: 1384256-35-2
(Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane

: 1384256-34-1
(Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 17h;
DOI:10.1016/j.tet.2012.04.117

Reference yield:

: 140-29-4
phenylacetonitrile

: 1384256-34-1
(Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane

Guidance literature:: Multi-step reaction with 4 steps

1: water; O,O-Diethyl hydrogen phosphorodithioate / 5 h / 85 - 90 °C

2: tetrahydrofuran / 16 h / 80 °C

3: triethylamine / dichloromethane / 19.75 h / 20 °C / Inert atmosphere; Cooling with ice

4: triethylamine / dichloromethane / 17 h / 20 °C

With water; O,O-Diethyl hydrogen phosphorodithioate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2012.04.117

Reference yield:

: 645-54-5
2-phenylthioacetamide

: 1384256-34-1
(Z)-1-acetyl-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-diazinane

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 16 h / 80 °C

2: triethylamine / dichloromethane / 19.75 h / 20 °C / Inert atmosphere; Cooling with ice

3: triethylamine / dichloromethane / 17 h / 20 °C

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2012.04.117