C₇H₉NO

Base Information

• Chemical Name: C₇H₉NO
• CAS No.: 1352834-02-6
• Molecular Formula: C₇H₉NO
• Molecular Weight: 123.155
• Mol file: 1352834-02-6.mol

Synonyms:C₇H₉NO

Chemical Property of C₇H₉NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₇H₉NO

There total 4 articles about C₇H₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-cyclohex-3-enecarboxylic acid (5709-98-8) → C7H9NO (1352834-02-6)

Guidance literature:

With diphenyl phosphoryl azide; triethylamine; In toluene; at 20 - 95 ℃; for 0.583333h; Product distribution / selectivity; Reflux;

Reference yield:

C7H9N3O → C7H9NO (1352834-02-6)

Guidance literature:

In toluene; at 110 ℃; for 2.5h; Inert atmosphere;

DOI:10.1080/00397911.2020.1802760

Reference yield:

1,2,5,6-tetrahydrobenzoic acid (4771-80-6) → C7H9NO (1352834-02-6)

Guidance literature:

Multi-step reaction with 3 steps

1: acetone / 0.42 h / 55 - 60 °C / Industry scale

2: hydrogenchloride / water; tert-butyl methyl ether / 20 - 25 °C

3: triethylamine; diphenyl phosphoryl azide / toluene / 0.58 h / 20 - 95 °C / Reflux

With hydrogenchloride; diphenyl phosphoryl azide; triethylamine; In tert-butyl methyl ether; water; acetone; toluene; 3: Curtius Rearrangement;

upstream raw materials:

(R)-cyclohex-3-enecarboxylic acid

1,2,5,6-tetrahydrobenzoic acid

Downstream raw materials:

D-3-aminohexanedioic acid

[(1R,3R,4R)-3-hydroxy-4-mercaptocyclohexyl]carbamic acid tert-butyl ester

14-O-{[(1R,2R,4R)-4-ethoxycarbonylamino-2-hydroxy-cyclohexyl-sulfanyl]-acetyl}-mutilin

14-O-{[(1R,2R,4R)-4-amino-2-hydroxy-cyclohexylsulfanyl]-acetyl}-mutilin hydrogenmaleate