ethyl 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarboxylate

Base Information

Chemical Name:ethyl 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarboxylate
CAS No.:409367-09-5
Molecular Formula:C₂₄H₂₉NO₄
Molecular Weight:395.499
Hs Code.:

Synonyms:ethyl 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarboxylate

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Chemical Property of ethyl 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarboxylate

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Technology Process of ethyl 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarboxylate

There total 1 articles about ethyl 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 30038-94-9
1-bromocyclopentane-carboxylic acid ethyl ester

: 131179-77-6
N-(3,5-dimethylphenyl)-4-hydroxyphenylacetamide

: 409367-09-5
ethyl 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarboxylate

Guidance literature:: With potassium carbonate; potassium iodide; In ethanol; for 25h; Heating;
DOI:10.1021/jm010358l

Reference yield: 91.0%

: 409367-09-5
ethyl 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarboxylate

: 170787-77-6
JP-7

Guidance literature:: With potassium hydroxide; In ethanol; for 50h; Heating;
DOI:10.1021/jm010358l

Reference yield:

: 409367-09-5
ethyl 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarboxylate

: 1-[4-(((3,5-dimethylanilino)carbonyl)methyl)phenoxy]cyclopentanecarbonyl-D-lysine

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / aq. KOH / ethanol / 50 h / Heating

2: 93.5 percent / HOBt*H₂O; EDC; NMM / dimethylformamide / 24 h / 20 °C

3: 92.4 percent / aq. LiOH / ethanol / 20 °C

4: 84.6 percent / H₂ / 10 percent Pd/C / ethanol

With 4-methyl-morpholine; potassium hydroxide; lithium hydroxide; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 10 percent Pd/C; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm010358l