Benzeneacetamide,N-[(5R,6R)-2-(1-methylethylidene)-3,7-dioxo-4-thia-1-azabicyclo[3.2.0]hept-6-yl]-

Base Information

Chemical Name:Benzeneacetamide,N-[(5R,6R)-2-(1-methylethylidene)-3,7-dioxo-4-thia-1-azabicyclo[3.2.0]hept-6-yl]-
CAS No.:17276-73-2
Molecular Formula:C₁₆H₁₆N₂O₃S
Molecular Weight:316.381
Hs Code.:

Synonyms:Acetamide,N-(2-isopropylidene-3,7-dioxo-4-thia-1-azabicyclo[3.2.0]hept-6-yl)-2-phenyl-(7CI,8CI); Benzeneacetamide,N-[2-(1-methylethylidene)-3,7-dioxo-4-thia-1-azabicyclo[3.2.0]hept-6-yl]-,(5R-trans)-; 4-Thia-1-azabicyclo[3.2.0]heptane-3,7-dione,2-isopropylidene-6-(2-phenylacetamido)-; Anhydropenicillin G; Penicillin G,anhydro-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzeneacetamide,N-[(5R,6R)-2-(1-methylethylidene)-3,7-dioxo-4-thia-1-azabicyclo[3.2.0]hept-6-yl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzeneacetamide,N-[(5R,6R)-2-(1-methylethylidene)-3,7-dioxo-4-thia-1-azabicyclo[3.2.0]hept-6-yl]-

There total 4 articles about Benzeneacetamide,N-[(5R,6R)-2-(1-methylethylidene)-3,7-dioxo-4-thia-1-azabicyclo[3.2.0]hept-6-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113-98-4
Penicillin G potassium

: 17276-73-2
N-((5R)-2-isopropylidene-3,7-dioxo-(5rH)-4-thia-1-aza-bicyclo[3.2.0]hept-6t-yl)-2-phenyl-acetamide

Guidance literature:: With pyridine; thionyl chloride; In dichloromethane;
DOI:10.1139/v68-417

Reference yield:

: 47579-62-4
1β-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid N'-isopropyl-hydrazide

: 17276-73-2
N-((5R)-2-isopropylidene-3,7-dioxo-(5rH)-4-thia-1-aza-bicyclo[3.2.0]hept-6t-yl)-2-phenyl-acetamide

Guidance literature:: With pyridine; phosphoric acid; In 1,4-dioxane; for 16h; Heating;
DOI:10.1039/P19720000929

Reference yield:

: 34104-15-9
penicillin G 1-oxide

: 17276-73-2
N-((5R)-2-isopropylidene-3,7-dioxo-(5rH)-4-thia-1-aza-bicyclo[3.2.0]hept-6t-yl)-2-phenyl-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: (i) ClCO₂Et, CHCl₃, (ii) /BRN= 1209233/, H₂O

2: Py, H₃PO₄ / dioxane / 16 h / Heating

With pyridine; phosphoric acid; In 1,4-dioxane;
DOI:10.1039/P19720000929