N-benzyl-N-crotonamide

Base Information

Chemical Name:N-benzyl-N-crotonamide
CAS No.:95712-46-2
Molecular Formula:C₁₆H₁₉NO₂
Molecular Weight:257.332
Hs Code.:

N-benzyl-N-<pent-2(E)-enal-5-yl>crotonamide

Synonyms:N-benzyl-N-crotonamide

Suppliers and Price of N-benzyl-N-crotonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-crotonamide

Chemical Property:

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Technology Process of N-benzyl-N-crotonamide

There total 13 articles about N-benzyl-N-crotonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95712-44-0
N-benzyl-N-<1-methoxymethyloxypent-2(Z)-en-5-yl>crotonamide

: 95712-46-2
N-benzyl-N-crotonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂SO₄ / ethanol / 9 h / Heating

2: oxalyl chloride, DMSO / CH₂Cl₂ / 1 h / -78 °C

3: CH₂Cl₂ / 11 h / Heating

With oxalyl dichloride; sulfuric acid; dimethyl sulfoxide; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)90579-4

Reference yield:

: 95712-43-9
N-benzyl-N-(5-(methoxymethoxy)pent-3(Z)-enyl)amine

: 95712-46-2
N-benzyl-N-crotonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / Et₃N, ethylchloroformate / CH₂Cl₂ / 6.5 h / Ambient temperature

2: 95 percent / H₂SO₄ / ethanol / 9 h / Heating

3: oxalyl chloride, DMSO / CH₂Cl₂ / 1 h / -78 °C

4: CH₂Cl₂ / 11 h / Heating

With oxalyl dichloride; sulfuric acid; chloroformic acid ethyl ester; dimethyl sulfoxide; triethylamine; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)90579-4

Reference yield:

: 95712-41-7
1-methoxymethyloxypent-2(Z)-ene-5-ol

: 95712-46-2
N-benzyl-N-crotonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / pyridine / CH₂Cl₂ / 12 h / -15 °C

2: 88 percent / NaI / dimethylsulfoxide / 20 h / Ambient temperature

3: 85 percent / Et₃N, ethylchloroformate / CH₂Cl₂ / 6.5 h / Ambient temperature

4: 95 percent / H₂SO₄ / ethanol / 9 h / Heating

5: oxalyl chloride, DMSO / CH₂Cl₂ / 1 h / -78 °C

6: CH₂Cl₂ / 11 h / Heating

With pyridine; oxalyl dichloride; sulfuric acid; chloroformic acid ethyl ester; dimethyl sulfoxide; triethylamine; sodium iodide; In ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(01)90579-4