C₅₀H₈₈O₁₂Si₃

Base Information

Chemical Name:C₅₀H₈₈O₁₂Si₃
CAS No.:1338704-35-0
Molecular Formula:C₅₀H₈₈O₁₂Si₃
Molecular Weight:965.498
Hs Code.:

C<sub>50</sub>H<sub>88</sub>O<sub>12</sub>Si<sub>3</sub>

Synonyms:C₅₀H₈₈O₁₂Si₃

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Chemical Property of C₅₀H₈₈O₁₂Si₃

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Technology Process of C₅₀H₈₈O₁₂Si₃

There total 21 articles about C₅₀H₈₈O₁₂Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338704-11-2
C₅₀H₈₆O₁₂Si₃

: 1338704-35-0
C₅₀H₈₈O₁₂Si₃

: C₅₀H₈₈O₁₂Si₃

Guidance literature:: C₅₀H₈₆O₁₂Si₃; With diethyl methoxy borane; In tetrahydrofuran; methanol; at -78 ℃; for 0.5h;

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at -78 - 0 ℃; optical yield given as %de;
DOI:10.1021/ol2024289

Reference yield:

: C₁₂H₂₂OS₂

: 1338704-35-0
C₅₀H₈₈O₁₂Si₃

: C₅₀H₈₈O₁₂Si₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

1.2: 1 h / -78 °C

2.1: water; iodine; sodium hydrogencarbonate / acetonitrile / 0.08 h / 0 - 25 °C

3.1: sodium tetrahydroborate; diethyl methoxy borane / tetrahydrofuran; methanol / -78 - 0 °C

4.1: manganese(IV) oxide / dichloromethane / 3 h / 25 °C

5.1: 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; acetic acid / toluene / 72 h / 0 °C

6.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C

7.1: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

7.2: 1.5 h / -78 °C

8.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.5 h / -78 °C

8.2: -78 - 0 °C

With 2,6-dimethylpyridine; manganese(IV) oxide; sodium tetrahydroborate; 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; diethyl methoxy borane; phenylborondichloride; water; iodine; tert.-butyl lithium; sodium hydrogencarbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; toluene; acetonitrile; pentane; 7.1: Aldol addition / 7.2: Aldol addition;
DOI:10.1021/ol2024289

Reference yield:

: 1095272-57-3
C₂₃H₄₀O₇Si₂

: 1338704-35-0
C₅₀H₈₈O₁₂Si₃

: C₅₀H₈₈O₁₂Si₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

1.2: 1.5 h / -78 °C

2.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.5 h / -78 °C

2.2: -78 - 0 °C

With diethyl methoxy borane; phenylborondichloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; 1.1: Aldol addition / 1.2: Aldol addition;
DOI:10.1021/ol2024289