Diphenylvinylidene-[2-(1-{[1-naphthalen-1-yl-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine

Base Information

• Chemical Name: Diphenylvinylidene-[2-(1-{[1-naphthalen-1-yl-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine
• CAS No.: 274917-39-4
• Molecular Formula: C₃₃H₂₆N₂
• Molecular Weight: 450.583
• Mol file: 274917-39-4.mol

Synonyms:Diphenylvinylidene-[2-(1-{[1-naphthalen-1-yl-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine

Chemical Property of Diphenylvinylidene-[2-(1-{[1-naphthalen-1-yl-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Diphenylvinylidene-[2-(1-{[1-naphthalen-1-yl-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine

There total 4 articles about Diphenylvinylidene-[2-(1-{[1-naphthalen-1-yl-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenyl ketene (525-06-4) + C22H25N2P → Diphenylvinylidene-[2-(1-{[1-naphthalen-1-yl-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine (274917-39-4)

Guidance literature:

In toluene; at 25 ℃; for 1h;

DOI:10.1021/jo991826q

Reference yield:

1-naphthaldehyde (66-77-3) → Diphenylvinylidene-[2-(1-{[1-naphthalen-1-yl-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine (274917-39-4)

Guidance literature:

Multi-step reaction with 3 steps

1: MgSO₄ / diethyl ether / 12 h / 25 °C

2: toluene / 20 °C

3: toluene / 1 h / 25 °C

With magnesium sulfate; In diethyl ether; toluene; 1: Condensation / 2: Addition / 3: Addition;

DOI:10.1021/jo991826q

Reference yield:

1-(o-azidophenyl)ethylamine (146954-07-6) → Diphenylvinylidene-[2-(1-{[1-naphthalen-1-yl-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine (274917-39-4)

Guidance literature:

Multi-step reaction with 3 steps

1: MgSO₄ / diethyl ether / 12 h / 25 °C

2: toluene / 20 °C

3: toluene / 1 h / 25 °C

With magnesium sulfate; In diethyl ether; toluene; 1: Condensation / 2: Addition / 3: Addition;

DOI:10.1021/jo991826q

upstream raw materials:

diphenyl ketene

1-naphthaldehyde

1-(o-azidophenyl)ethylamine

[1-(2-Azido-phenyl)-ethyl]-[1-naphthalen-1-yl-meth-(E)-ylidene]-amine