(2S,4aS,7R,8aR)-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine

Base Information

• Chemical Name: (2S,4aS,7R,8aR)-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine
• CAS No.: 853180-76-4
• Molecular Formula: C₁₇H₂₉NO
• Molecular Weight: 263.423

Synonyms:(2S,4aS,7R,8aR)-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine

Chemical Property of (2S,4aS,7R,8aR)-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine

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Technology Process of (2S,4aS,7R,8aR)-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine

There total 1 articles about (2S,4aS,7R,8aR)-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-cyclohexene-1-carboxaldehyde (1192-88-7) + (-)-aminomenthol (55179-51-6) → (2S,4aS,7R,8aR)-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine (853180-76-4)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1021/jo050360a

Reference yield: 91.0%

(2S,4aS,7R,8aR)-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine (853180-76-4) + propargyl bromide (106-96-7) → (2S,4aS,7R,8aR)-N-propargyl-2-(cyclohexen-1-yl)-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine (1374023-18-3)

Guidance literature:

With potassium carbonate; In acetonitrile; Reflux;

DOI:10.1002/ejoc.201101462

Reference yield: 89.0%

(2S,4aS,7R,8aR)-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine (853180-76-4) + 1-Bromo-2-butyne (3355-28-0) → (2S,4aS,7R,8aR)-N-(2-butyn-1-yl)-2-(cyclohexen-1-yl)-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine (1374023-19-4)

Guidance literature:

With potassium carbonate; In acetonitrile; Reflux;

DOI:10.1002/ejoc.201101462

upstream raw materials:

1-cyclohexene-1-carboxaldehyde

(-)-aminomenthol

Downstream raw materials:

(2S,4aS,7R,8aR)-N-acryloyl-2-cyclohexen-1-yl-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine

(4S,5R)-N-(8-mentholyl)-4-methyl-2-azaspiro[4,5]dec-6-ene

(3aR,5aS)-2-tosyloctahydro-1H-indeno[1-c]pyrrol-5(5aH)-one

(2S,4aS,7R,8aR)-N-(2-butyn-1-yl)-2-(cyclohexen-1-yl)-4,4,7-trimethyloctahydrobenz[e][1,3]oxazine

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