C₃₉H₆₇BrO₄Si₃

Base Information

Chemical Name:C₃₉H₆₇BrO₄Si₃
CAS No.:1266178-34-0
Molecular Formula:C₃₉H₆₇BrO₄Si₃
Molecular Weight:764.119
Hs Code.:

C<sub>39</sub>H<sub>67</sub>BrO<sub>4</sub>Si<sub>3</sub>

Synonyms:C₃₉H₆₇BrO₄Si₃

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Chemical Property of C₃₉H₆₇BrO₄Si₃

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Technology Process of C₃₉H₆₇BrO₄Si₃

There total 4 articles about C₃₉H₆₇BrO₄Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1266178-98-6
C₃₀H₄₇BrO₄Si₂

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1266178-34-0
C₃₉H₆₇BrO₄Si₃

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201005850

Reference yield:

: C₃₀H₄₆O₃Si₂

: 1266178-34-0
C₃₉H₆₇BrO₄Si₃

Guidance literature:: Multi-step reaction with 4 steps

1: silver nitrate; calcium carbonate / water; acetone / 4 h / Inert atmosphere; Darkness

2: N-Bromosuccinimide; water / 48 h / 10 °C / Inert atmosphere; Darkness

3: water; sodium hydrogencarbonate / methanol / Inert atmosphere

4: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; N-Bromosuccinimide; water; sodium hydrogencarbonate; silver nitrate; calcium carbonate; In methanol; dichloromethane; water; acetone;
DOI:10.1002/anie.201005850

Reference yield:

: 1266178-31-7
C₃₀H₄₆O₃Si₂

: 1266178-34-0
C₃₉H₆₇BrO₄Si₃

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; water / 48 h / 10 °C / Inert atmosphere; Darkness

2: water; sodium hydrogencarbonate / methanol / Inert atmosphere

3: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; N-Bromosuccinimide; water; sodium hydrogencarbonate; In methanol; dichloromethane;
DOI:10.1002/anie.201005850