2-{(1E)-2-[(5-{N-[5-(N-aminocarbamoyl)pentyl]carbamoyl}(2-pyridyl))amino]-2-azavinyl}benzenesulfonic acid

Base Information

Chemical Name:2-{(1E)-2-[(5-{N-[5-(N-aminocarbamoyl)pentyl]carbamoyl}(2-pyridyl))amino]-2-azavinyl}benzenesulfonic acid
CAS No.:848083-92-1
Molecular Formula:C₁₉H₂₄N₆O₅S
Molecular Weight:448.503
Hs Code.:

Synonyms:2-{(1E)-2-[(5-{N-[5-(N-aminocarbamoyl)pentyl]carbamoyl}(2-pyridyl))amino]-2-azavinyl}benzenesulfonic acid

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Chemical Property of 2-{(1E)-2-[(5-{N-[5-(N-aminocarbamoyl)pentyl]carbamoyl}(2-pyridyl))amino]-2-azavinyl}benzenesulfonic acid

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Technology Process of 2-{(1E)-2-[(5-{N-[5-(N-aminocarbamoyl)pentyl]carbamoyl}(2-pyridyl))amino]-2-azavinyl}benzenesulfonic acid

There total 2 articles about 2-{(1E)-2-[(5-{N-[5-(N-aminocarbamoyl)pentyl]carbamoyl}(2-pyridyl))amino]-2-azavinyl}benzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 848083-91-0
sodium 2-[(1E)-2-aza-2-({5-[N-(5-{N-[(tert-butoxy)-carbonylamino]carbamoyl}pentyl)carbamoyl](2-pyridyl)}amino)vinyl]benzenesulfonate

: 848083-92-1
2-{(1E)-2-[(5-{N-[5-(N-aminocarbamoyl)pentyl]carbamoyl}(2-pyridyl))amino]-2-azavinyl}benzenesulfonic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.166667h;

Reference yield:

: 848083-89-6
N-[(tert-butoxy)carbonylamino]-6-[(fluoren-9-ylmethoxy)carbonylamino]hexanamide

: 848083-92-1
2-{(1E)-2-[(5-{N-[5-(N-aminocarbamoyl)pentyl]carbamoyl}(2-pyridyl))amino]-2-azavinyl}benzenesulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / N,N-dimethyl-formamide / 0.33 h / 20 °C

2: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

3: trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C

With piperidine; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield: 63.0%

: 848083-92-1
2-{(1E)-2-[(5-{N-[5-(N-aminocarbamoyl)pentyl]carbamoyl}(2-pyridyl))amino]-2-azavinyl}benzenesulfonic acid

: 108-24-7
acetic anhydride

: 848084-07-1
C₂₁H₂₆N₆O₆S

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;