(E)-3-(1,3-dioxan-2-yl)-2-nitro-1-(1-phenylsulfonyl-3-pyrrolyl)-1-propene

Base Information

Chemical Name:(E)-3-(1,3-dioxan-2-yl)-2-nitro-1-(1-phenylsulfonyl-3-pyrrolyl)-1-propene
CAS No.:146073-24-7
Molecular Formula:C₁₇H₁₈N₂O₆S
Molecular Weight:378.406
Hs Code.:

Synonyms:(E)-3-(1,3-dioxan-2-yl)-2-nitro-1-(1-phenylsulfonyl-3-pyrrolyl)-1-propene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(1,3-dioxan-2-yl)-2-nitro-1-(1-phenylsulfonyl-3-pyrrolyl)-1-propene

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Technology Process of (E)-3-(1,3-dioxan-2-yl)-2-nitro-1-(1-phenylsulfonyl-3-pyrrolyl)-1-propene

There total 1 articles about (E)-3-(1,3-dioxan-2-yl)-2-nitro-1-(1-phenylsulfonyl-3-pyrrolyl)-1-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 88075-95-0
1-(phenylsulfonyl)-1H-pyrrole-3-carbaldehyde

: 146073-16-7
2-(2-nitroethyl)-1,3-dioxane

: 146073-24-7
(E)-3-(1,3-dioxan-2-yl)-2-nitro-1-(1-phenylsulfonyl-3-pyrrolyl)-1-propene

Guidance literature:: With ammonium acetate; In acetonitrile; for 15h; Heating;
DOI:10.1248/cpb.40.2344

Reference yield:

: 146073-24-7
(E)-3-(1,3-dioxan-2-yl)-2-nitro-1-(1-phenylsulfonyl-3-pyrrolyl)-1-propene

: 1-Benzenesulfonyl-3-(3-[1,3]dioxan-2-yl-2-nitro-propyl)-1H-pyrrole

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 1h; Ambient temperature;
DOI:10.1248/cpb.40.2344

Reference yield:

: 146073-24-7
(E)-3-(1,3-dioxan-2-yl)-2-nitro-1-(1-phenylsulfonyl-3-pyrrolyl)-1-propene

: 56995-12-1
1-benzenesulfonyl-5-methoxy-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / ethanol / 1 h / Ambient temperature

2: 1.) NaOMe, 2.) TiCl₃, aq. NH₄OAc / 1.) EtOH, RT, 5 min, 2.) EtOH, RT, 3 h

3: 89 percent / p-TsOH*H₂O / methanol / 1 h / Heating

With sodium tetrahydroborate; titanium(III) chloride; ammonium acetate; sodium methylate; toluene-4-sulfonic acid; In methanol; ethanol;
DOI:10.1248/cpb.40.2344