2-[(3-benzyloxycarbonylaminopropionyl)trimethylsilylmethylamino]-4-methylpentanoic acid methyl ester

Base Information

Chemical Name:2-[(3-benzyloxycarbonylaminopropionyl)trimethylsilylmethylamino]-4-methylpentanoic acid methyl ester
CAS No.:916049-34-8
Molecular Formula:C₂₂H₃₆N₂O₅Si
Molecular Weight:436.624
Hs Code.:

Synonyms:2-[(3-benzyloxycarbonylaminopropionyl)trimethylsilylmethylamino]-4-methylpentanoic acid methyl ester

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Chemical Property of 2-[(3-benzyloxycarbonylaminopropionyl)trimethylsilylmethylamino]-4-methylpentanoic acid methyl ester

Chemical Property:

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Technology Process of 2-[(3-benzyloxycarbonylaminopropionyl)trimethylsilylmethylamino]-4-methylpentanoic acid methyl ester

There total 5 articles about 2-[(3-benzyloxycarbonylaminopropionyl)trimethylsilylmethylamino]-4-methylpentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 916049-31-5
4-methyl-2-[(4-nitrobenzenesulfonyl)trimethylsilanylmethylamino]pentanoic acid methyl ester

: 916049-34-8
2-[(3-benzyloxycarbonylaminopropionyl)trimethylsilylmethylamino]-4-methylpentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; benzenethiol / acetonitrile / 12 h / 20 °C

2: 1.82 g / CH₂Cl₂ / 12 h / 20 °C

With potassium carbonate; thiophenol; In dichloromethane; acetonitrile;
DOI:10.1021/ja064737l

Reference yield:

: 2666-93-5
(S)-Leu-OMe

: 916049-34-8
2-[(3-benzyloxycarbonylaminopropionyl)trimethylsilylmethylamino]-4-methylpentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / CH₂Cl₂ / 12 h / 20 °C

2: 4.6 g / potassium iodide; potassium carbonate / dimethylformamide / 12 h / 60 °C

3: potassium carbonate; benzenethiol / acetonitrile / 12 h / 20 °C

4: 1.82 g / CH₂Cl₂ / 12 h / 20 °C

With potassium carbonate; thiophenol; triethylamine; potassium iodide; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja064737l

Reference yield:

: 2304-94-1
3-(benzyloxycarbonylamino)propanoic acid

: 916049-34-8
2-[(3-benzyloxycarbonylaminopropionyl)trimethylsilylmethylamino]-4-methylpentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / CH₂Cl₂ / 0.42 h / -15 °C

2: 1.82 g / CH₂Cl₂ / 12 h / 20 °C

With 4-methyl-morpholine; In dichloromethane;
DOI:10.1021/ja064737l