C₁₆H₃₆N⁽¹⁺⁾*C₂₂H₂₀NO₇^(1-)

Base Information

Chemical Name:C₁₆H₃₆N⁽¹⁺⁾*C₂₂H₂₀NO₇^(1-)
CAS No.:1401528-98-0
Molecular Formula:C₁₆H₃₆N*C₂₂H₂₀NO₇
Molecular Weight:652.872
Hs Code.:

C<sub>16</sub>H<sub>36</sub>N<sup>(1+)</sup>*C<sub>22</sub>H<sub>20</sub>NO<sub>7</sub><sup>(1-)</sup>

Synonyms:C₁₆H₃₆N⁽¹⁺⁾*C₂₂H₂₀NO₇^(1-)

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Chemical Property of C₁₆H₃₆N⁽¹⁺⁾*C₂₂H₂₀NO₇^(1-)

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Technology Process of C₁₆H₃₆N⁽¹⁺⁾*C₂₂H₂₀NO₇^(1-)

There total 5 articles about C₁₆H₃₆N⁽¹⁺⁾*C₂₂H₂₀NO₇^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 120404-76-4
2-(hydroxymethyl)-1,5-bis((4-methoxybenzyl)oxy)pyridin-4(1H)-one

: 1643-19-2
tetrabutylammomium bromide

: 1401528-98-0
C₁₆H₃₆N⁽¹⁺⁾*C₂₂H₂₀NO₇^(1-)

Guidance literature:: 2-(hydroxymethyl)-1,5-bis((4-methoxybenzyl)oxy)pyridin-4(1H)-one; tetrabutylammomium bromide; With sodium hypochlorite; sodium hydrogencarbonate; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In dichloromethane; water; at 0 - 20 ℃; for 1.5h;

With hydrogenchloride; In dichloromethane; water; pH=6 - 7;

With sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; sodium chloride; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; at 20 ℃; for 1h;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1401528-98-0
C₁₆H₃₆N⁽¹⁺⁾*C₂₂H₂₀NO₇^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

2.1: hydroxylamine hydrochloride; pyridine / 70 - 75 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C

4.1: sodium hydrogencarbonate; sodium hypochlorite; sodium bromide / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 1.5 h / 0 - 20 °C

4.2: pH 6 - 7

4.3: 1 h / 20 °C

With pyridine; sodium hypochlorite; hydroxylamine hydrochloride; sodium hydrogencarbonate; potassium carbonate; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 120404-75-3
1-hydroxy-2-hydroxymethyl-5-(4-methoxybenzyloxy)-4-pyridone

: 1401528-98-0
C₁₆H₃₆N⁽¹⁺⁾*C₂₂H₂₀NO₇^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C

2.1: sodium hydrogencarbonate; sodium hypochlorite; sodium bromide / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 1.5 h / 0 - 20 °C

2.2: pH 6 - 7

2.3: 1 h / 20 °C

With sodium hypochlorite; sodium hydrogencarbonate; potassium carbonate; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In dichloromethane; water; N,N-dimethyl-formamide;