C₅₈H₆₀N₄O₄

Base Information

Chemical Name:C₅₈H₆₀N₄O₄
CAS No.:1428428-13-0
Molecular Formula:C₅₈H₆₀N₄O₄
Molecular Weight:877.139
Hs Code.:

C<sub>58</sub>H<sub>60</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₅₈H₆₀N₄O₄

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Chemical Property of C₅₈H₆₀N₄O₄

Chemical Property:

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Technology Process of C₅₈H₆₀N₄O₄

There total 16 articles about C₅₈H₆₀N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₄₀N₂O₃

: 160446-35-5
3-(1H-1-triphenylmethylimidazol-4-yl)propanoic acid

: 1428428-13-0
C₅₈H₆₀N₄O₄

Guidance literature:: 3-(1H-1-triphenylmethylimidazol-4-yl)propanoic acid; With pivaloyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

C₃₃H₄₀N₂O₃; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol400469w

Reference yield:

: C₃₄H₃₉NO₃Si

: 1428428-13-0
C₅₈H₆₀N₄O₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 12 h / Inert atmosphere; Reflux

3.1: lithium borohydride / ethanol / 4 h / Inert atmosphere

4.1: palladium 10% on activated carbon; ammonium formate / methanol / 12.5 h / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / Inert atmosphere

6.1: sodium hydride / N,N-dimethyl-formamide; tetrahydrofuran; mineral oil / 2 h / 0 - 60 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

8.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

9.1: copper(II) sulfate / toluene / 16 h / 20 °C / Inert atmosphere

10.1: N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran; chlorobenzene / 0.5 h / 20 - 110 °C / Inert atmosphere

11.1: hydrogenchloride / Inert atmosphere

12.1: N-ethyl-N,N-diisopropylamine; pivaloyl chloride / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

12.2: 0.5 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium borohydride; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; ammonium formate; pivaloyl chloride; sodium hydride; Dess-Martin periodane; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; chlorobenzene; toluene; mineral oil; 10.1: |Grignard Reaction;
DOI:10.1021/ol400469w

Reference yield:

: C₂₀H₂₃NO₄

: 1428428-13-0
C₅₈H₆₀N₄O₄

Guidance literature:: Multi-step reaction with 14 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

3.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

4.1: tetrahydrofuran / 12 h / Inert atmosphere; Reflux

5.1: lithium borohydride / ethanol / 4 h / Inert atmosphere

6.1: palladium 10% on activated carbon; ammonium formate / methanol / 12.5 h / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / Inert atmosphere

8.1: sodium hydride / N,N-dimethyl-formamide; tetrahydrofuran; mineral oil / 2 h / 0 - 60 °C / Inert atmosphere

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

10.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

11.1: copper(II) sulfate / toluene / 16 h / 20 °C / Inert atmosphere

12.1: N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran; chlorobenzene / 0.5 h / 20 - 110 °C / Inert atmosphere

13.1: hydrogenchloride / Inert atmosphere

14.1: N-ethyl-N,N-diisopropylamine; pivaloyl chloride / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

14.2: 0.5 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium borohydride; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; ammonium formate; pivaloyl chloride; sodium hydride; Dess-Martin periodane; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; chlorobenzene; toluene; mineral oil; 12.1: |Grignard Reaction;
DOI:10.1021/ol400469w