o-(tributylstannylmethyl)benzylideneaniline

Base Information

Chemical Name:o-(tributylstannylmethyl)benzylideneaniline
CAS No.:1619923-74-8
Molecular Formula:C₂₆H₃₉NSn
Molecular Weight:484.312
Hs Code.:

Synonyms:o-(tributylstannylmethyl)benzylideneaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-(tributylstannylmethyl)benzylideneaniline

Chemical Property:

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Technology Process of o-(tributylstannylmethyl)benzylideneaniline

There total 4 articles about o-(tributylstannylmethyl)benzylideneaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 62-53-3
aniline

: o-(tributylstannylmethyl)benzaldehyde

: 1619923-74-8
o-(tributylstannylmethyl)benzylideneaniline

Guidance literature:: In benzene; at 20 ℃; for 48h; Molecular sieve;
DOI:10.1016/j.tetlet.2014.05.107

Reference yield:

: 113431-27-9
o-(hydroxymethyl)benzyltributylstannane

: 1619923-74-8
o-(tributylstannylmethyl)benzylideneaniline

Guidance literature:: Multi-step reaction with 2 steps

1: dipyridinium dichromate; aluminum oxide / dichloromethane / 3.5 h / 20 °C

2: benzene / 48 h / 20 °C / Molecular sieve

With aluminum oxide; dipyridinium dichromate; In dichloromethane; benzene;
DOI:10.1016/j.tetlet.2014.05.107

Reference yield:

: 1461-22-9
tributyltin chloride

: 1619923-74-8
o-(tributylstannylmethyl)benzylideneaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / Reflux

1.2: 1 h / 20 °C

2.1: dipyridinium dichromate; aluminum oxide / dichloromethane / 3.5 h / 20 °C

3.1: benzene / 48 h / 20 °C / Molecular sieve

With aluminum oxide; dipyridinium dichromate; n-butyllithium; In diethyl ether; hexane; dichloromethane; benzene;
DOI:10.1016/j.tetlet.2014.05.107