C₂₁H₃₁⁽²⁾H₆O₆P

Base Information

• Chemical Name: C₂₁H₃₁⁽²⁾H₆O₆P
• CAS No.: 217471-20-0
• Molecular Formula: C₂₁H₃₇O₆P
• Molecular Weight: 422.447
• Mol file: 217471-20-0.mol

Synonyms:C₂₁H₃₁⁽²⁾H₆O₆P

Chemical Property of C₂₁H₃₁⁽²⁾H₆O₆P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₁H₃₁⁽²⁾H₆O₆P

There total 6 articles about C₂₁H₃₁⁽²⁾H₆O₆P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

phosphonic acid diethyl ester (762-04-9) + C17H22(2)H6O3 (217471-19-7) → C21H31(2)H6O6P (217471-20-0)

Guidance literature:

With triethylamine; In tetrachloromethane; at -15 - 25 ℃; for 16.25h;

DOI:10.1002/(SICI)1099-1344(1998100)41:10<885::AID-JLCR139>3.0.CO;2-6

Reference yield:

1,3-dimethoxy-2-hydroxy-benzene (91-10-1) → C21H31(2)H6O6P (217471-20-0)

Guidance literature:

Multi-step reaction with 3 steps

1: deuterium oxide / toluene / 0.33 h

2: 11.5 g / O-deuterio-trifluoromethanesulfonic acid / 72 h / 20 - 25 °C

3: 70 percent / triethylamine / CCl₄ / 16.25 h / -15 - 25 °C

With water-d2; triethylamine; In tetrachloromethane; toluene; 1: deuteration / 2: Alkylation / 3: Oxidation;

DOI:10.1002/(SICI)1099-1344(1998100)41:10<885::AID-JLCR139>3.0.CO;2-6

Reference yield:

ethyl heptanoate (106-30-9) → C21H31(2)H6O6P (217471-20-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: magnesium; iodine / diethyl ether

1.2: 9.0 g / diethyl ether / 20 - 25 °C

2.1: deuterium oxide / toluene / 0.33 h / 20 - 25 °C

3.1: 11.5 g / O-deuterio-trifluoromethanesulfonic acid / 72 h / 20 - 25 °C

4.1: 70 percent / triethylamine / CCl₄ / 16.25 h / -15 - 25 °C

With iodine; water-d2; magnesium; triethylamine; In tetrachloromethane; diethyl ether; toluene; 1.1: Metallation / 1.2: Grignard reaction / 2.1: deuteration / 3.1: Alkylation / 4.1: Oxidation;

DOI:10.1002/(SICI)1099-1344(1998100)41:10<885::AID-JLCR139>3.0.CO;2-6

upstream raw materials:

phosphonic acid diethyl ester

C₁₇H₂₂⁽²⁾H₆O₃

1,3-dimethoxy-2-hydroxy-benzene

ethyl heptanoate

Downstream raw materials:

C₁₅H₁₉⁽²⁾H₅O₂

C₁₇H₂₂⁽²⁾H₆O₂