(E)-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pent-2-en-1-ol

Base Information

Chemical Name:(E)-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pent-2-en-1-ol
CAS No.:610272-80-5
Molecular Formula:C₁₃H₁₈O₃
Molecular Weight:230.221
Hs Code.:

(E)-5-(3,4-dimethoxyphenyl)-3-[2H<sub>3</sub>]methyl-2-[1,1,2,4,4-2H<sub>5</sub>]pent-2-en-1-ol

Synonyms:(E)-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pent-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pent-2-en-1-ol

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Technology Process of (E)-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pent-2-en-1-ol

There total 2 articles about (E)-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pent-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 610272-79-2
ethyl (E)-3-[2H₃]methyl-4-(3,4-dimethoxyphenyl)-[2,4,4-2H₃]but-2-enoate

: 610272-80-5
(E)-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pent-2-en-1-ol

Guidance literature:: With lithium aluminium deuteride; In diethyl ether; at 0 ℃; for 2.5h;
DOI:10.1016/S0040-4020(03)00983-9

Reference yield:

: 207979-18-8
(3,4-dimethoxyphenyl)[1,1,3,3,3-2H₅]acetone

: 610272-80-5
(E)-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pent-2-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 1 h / 20 °C

1.2: 59 percent / tetrahydrofuran / 7 h / 20 °C

2.1: 74 percent / lithium aluminum deuteride / diethyl ether / 2.5 h / 0 °C

With lithium aluminium deuteride; sodium hydride; In tetrahydrofuran; diethyl ether; 1.1: Horner-Emmons reaction;
DOI:10.1016/S0040-4020(03)00983-9

Reference yield: 77.0%

: 610272-80-5
(E)-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pent-2-en-1-ol

: 610272-81-6
(2S,3S)-2,3-epoxy-5-(3,4-dimethoxyphenyl)-3-[2H₃]methyl-2-[1,1,2,4,4-2H₅]pentan-1-ol

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; In dichloromethane; at -25 ℃; for 1h;
DOI:10.1016/S0040-4020(03)00983-9