C₁₅H₂₁NO₃

Base Information

Chemical Name:C₁₅H₂₁NO₃
CAS No.:1319734-50-3
Molecular Formula:C₁₅H₂₁NO₃
Molecular Weight:263.337
Hs Code.:

C<sub>15</sub>H<sub>21</sub>NO<sub>3</sub>

Synonyms:C₁₅H₂₁NO₃

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Chemical Property of C₁₅H₂₁NO₃

Chemical Property:

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Technology Process of C₁₅H₂₁NO₃

There total 6 articles about C₁₅H₂₁NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₈H₁₂O₃

: 100-46-9
benzylamine

: 1319734-50-3
C₁₅H₂₁NO₃

Guidance literature:: C₈H₁₂O₃; benzylamine; With sodium hydroxide; In water; for 2.5h; Reflux;

With sodium hydroxide; In water; at 20 ℃;

With hydrogenchloride; In water; pH=4 - 5; regioselective reaction;
DOI:10.1016/j.bmc.2011.05.022

Reference yield:

: 152972-34-4
C₈H₁₄O

: 1319734-50-3
C₁₅H₂₁NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butylhydroperoxide; titanium(IV) isopropoxide; diethyl (2S,3S)-tartrate / octane; dichloromethane / 3 h / -30 - -20 °C / Molecular sieve; Inert atmosphere

1.2: 1.5 h / -30 - -20 °C

2.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 20 °C

3.1: sodium dihydrogenphosphate; sodium hypochlorite; 2-methyl-but-2-ene / water; acetonitrile / 20 - 25 °C

3.2: 20 °C

3.3: pH 3

4.1: sodium hydroxide / water / 2.5 h / Reflux

4.2: 20 °C

4.3: pH 4 - 5

With tert.-butylhydroperoxide; sodium hypochlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; diethyl (2S,3S)-tartrate; titanium(IV) isopropoxide; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; sodium hydroxide; In octane; dichloromethane; water; acetonitrile; 1.1: Sharpless epoxidation;
DOI:10.1016/j.bmc.2011.05.022

Reference yield:

: C₈H₁₂O₂

: 1319734-50-3
C₁₅H₂₁NO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium dihydrogenphosphate; sodium hypochlorite; 2-methyl-but-2-ene / water; acetonitrile / 20 - 25 °C

1.2: 20 °C

1.3: pH 3

2.1: sodium hydroxide / water / 2.5 h / Reflux

2.2: 20 °C

2.3: pH 4 - 5

With sodium hypochlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydroxide; In water; acetonitrile;
DOI:10.1016/j.bmc.2011.05.022