C₆₈H₁₁₉N₃O₅S₃Si

Base Information

Chemical Name:C₆₈H₁₁₉N₃O₅S₃Si
CAS No.:1338832-58-8
Molecular Formula:C₆₈H₁₁₉N₃O₅S₃Si
Molecular Weight:1182.99
Hs Code.:

C<sub>68</sub>H<sub>119</sub>N<sub>3</sub>O<sub>5</sub>S<sub>3</sub>Si

Synonyms:C₆₈H₁₁₉N₃O₅S₃Si

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Chemical Property of C₆₈H₁₁₉N₃O₅S₃Si

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Technology Process of C₆₈H₁₁₉N₃O₅S₃Si

There total 7 articles about C₆₈H₁₁₉N₃O₅S₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1338832-59-9
N-biotinyl-1-mercapto-3-(tert-butyl(diphenyl)silyloxy)propan-2-amine

: 144944-51-4,146491-00-1
rac-2,3-bis(octadecyloxy)propane-1-thiol

: 1338832-58-8
C₆₈H₁₁₉N₃O₅S₃Si

Guidance literature:: rac-2,3-bis(octadecyloxy)propane-1-thiol; With PTAD; In dichloromethane; acetonitrile; at 20 - 60 ℃; for 1.5h; Inert atmosphere;

N-biotinyl-1-mercapto-3-(tert-butyl(diphenyl)silyloxy)propan-2-amine; In dichloromethane; acetonitrile; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2011.07.089

Reference yield:

: 1278996-66-9
1-(benzylthio)-3-(tert-butyldiphenylsilyloxy)propan-2-ol

: 1338832-58-8
C₆₈H₁₁₉N₃O₅S₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

2.1: hydrazine hydrate / ethanol / 72 h / 20 °C / Reflux

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

4.1: ammonia; sodium / 2.5 h / -78 °C / Inert atmosphere

5.1: PTAD / dichloromethane; acetonitrile / 1.5 h / 20 - 60 °C / Inert atmosphere

5.2: 24 h / 20 °C / Inert atmosphere

With PTAD; di-isopropyl azodicarboxylate; ammonia; sodium; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1.1: Mitsunobu reaction;
DOI:10.1016/j.tet.2011.07.089

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1338832-58-8
C₆₈H₁₁₉N₃O₅S₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 72 h / 20 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

3.1: hydrazine hydrate / ethanol / 72 h / 20 °C / Reflux

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

5.1: ammonia; sodium / 2.5 h / -78 °C / Inert atmosphere

6.1: PTAD / dichloromethane; acetonitrile / 1.5 h / 20 - 60 °C / Inert atmosphere

6.2: 24 h / 20 °C / Inert atmosphere

With 1H-imidazole; PTAD; di-isopropyl azodicarboxylate; ammonia; sodium; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2.1: Mitsunobu reaction;
DOI:10.1016/j.tet.2011.07.089