N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine

Base Information

Chemical Name:N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine
CAS No.:174905-84-1
Molecular Formula:C₂₁H₂₉NO₃S
Molecular Weight:375.532
Hs Code.:

Synonyms:N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine

Suppliers and Price of N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine

There total 3 articles about N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 174905-82-9
N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzamide

: 174905-84-1
N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 10h; Heating;
DOI:10.3987/com-94-s7-1

Reference yield:

: 38228-27-2
N,N-diethyl-3,5-dimethoxybenzamide

: 174905-84-1
N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 1.) N,N,N',N'-tetramethylethylenediamine, sec-BuLi; 2.) sulfur / tetrahydrofuran; cyclohexane / 1.) -78 deg C, 30 min; 2.) -78 deg C, 2.5 h; 3.) 0 deg C, 2 h

2: 89 percent / LiAlH₄ / diethyl ether / 10 h / Heating

With lithium aluminium tetrahydride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; sulfur; In tetrahydrofuran; diethyl ether; cyclohexane;
DOI:10.3987/com-94-s7-1

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 174905-84-1
N,N-diethyl-3,5-dimethoxy-2-<<(4-methoxyphenyl)methyl>thio>benzenemethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 1.) N,N,N',N'-tetramethylethylenediamine, sec-BuLi; 2.) sulfur / tetrahydrofuran; cyclohexane / 1.) -78 deg C, 30 min; 2.) -78 deg C, 2.5 h; 3.) 0 deg C, 2 h

2: 89 percent / LiAlH₄ / diethyl ether / 10 h / Heating

With lithium aluminium tetrahydride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; sulfur; In tetrahydrofuran; diethyl ether; cyclohexane;
DOI:10.3987/com-94-s7-1