[Ru(η6-octamethylnaphthalene)(η6-hexamethylbenzene)]bis(tetraphenylborate)

Base Information

Chemical Name:[Ru(η6-octamethylnaphthalene)(η6-hexamethylbenzene)]bis(tetraphenylborate)
CAS No.:88946-88-7
Molecular Formula:2C₂₄H₂₀B*C₃₀H₄₂Ru
Molecular Weight:1142.2
Hs Code.:

Synonyms:[Ru(η6-octamethylnaphthalene)(η6-hexamethylbenzene)]bis(tetraphenylborate)

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Chemical Property of [Ru(η6-octamethylnaphthalene)(η6-hexamethylbenzene)]bis(tetraphenylborate)

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Technology Process of [Ru(η6-octamethylnaphthalene)(η6-hexamethylbenzene)]bis(tetraphenylborate)

There total 2 articles about [Ru(η6-octamethylnaphthalene)(η6-hexamethylbenzene)]bis(tetraphenylborate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: [RuCl₂(hexamethylbenzene)]2

: 18623-61-5
octamethylnaphthalene

: 143-66-8
sodium tetraphenyl borate

: 88946-88-7
[Ru(η6-octamethylnaphthalene)(η6-hexamethylbenzene)]bis(tetraphenylborate)

Guidance literature:: With AgBF₄; trifluoroacetic acid; In acetone; byproducts: AgCl; Ru-complex and AgBF4 were stirred vigorously together in acetone for about 15 min, filtered, filtrate evapd., C10Me8 and CF3COOH were added to the residue, mixt. was refluxed with stirring for 20 min; soln. was evapd. under vac., residue was thoroughly extd. with water, ext. filtered, excess NaBPh4 was added to the filtrate with stirring, after a few min mixt. was filtered, ppt. rinsed with water and Et2O, recrystd. from hot MeCN;

Reference yield:

: [Ru(η6-octamethylnaphthalene)(η6-hexamethylbenzene)]bis(hexafluorophosphate)

: 143-66-8
sodium tetraphenyl borate

: 88946-88-7
[Ru(η6-octamethylnaphthalene)(η6-hexamethylbenzene)]bis(tetraphenylborate)

Guidance literature:: In acetonitrile; an excess of NaBPh4 was added to a MeCN soln. of Ru-complex; ppt. was collected, rinsed with cold MeCN, recrystd. from hot MeCN; elem. anal.;