(6R,7R)-7-Amino-8-oxo-3-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

Base Information

Chemical Name:(6R,7R)-7-Amino-8-oxo-3-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid
CAS No.:55817-54-4
Molecular Formula:C₁₅H₁₄N₆O₃S₂
Molecular Weight:390.447
Hs Code.:

Synonyms:(6R,7R)-7-Amino-8-oxo-3-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

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Chemical Property of (6R,7R)-7-Amino-8-oxo-3-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

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Technology Process of (6R,7R)-7-Amino-8-oxo-3-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

There total 2 articles about (6R,7R)-7-Amino-8-oxo-3-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 957-68-6
7-Aminocephalosporanic acid

: 55817-54-4
(6R,7R)-7-Amino-8-oxo-3-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

Guidance literature:: With boron trifluoride; In acetonitrile; at 30 ℃; for 1.5h;
DOI:10.1248/cpb.33.5534

Reference yield:

: 55817-54-4
7-Amino-8-oxo-3-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

Guidance literature:: 7-Aminocephalosporansaeure, 5-Mercapto-1-phenyl-1H-tetrazol-BF3 * Et2O;

Reference yield:

: (Z)-4,5-bis(benzhydryloxy)-2-(1-(((carboxy(2-(tritylamino)thiazol-4-yl)methylene)amino)oxy)-2-methylpropyl)pyridine 1-oxide

: 55817-54-4
(6R,7R)-7-Amino-8-oxo-3-(1-phenyl-1H-tetrazol-5-ylsulfanylmethyl)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

: C₇₄H₆₂N₁₀O₈S₃

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 5.25h; Inert atmosphere;