O-(2,3,4,6-tetra-O-acetyl-D-glucopyranosylidene)amino N-phenylcarbamate

Base Information

Chemical Name:O-(2,3,4,6-tetra-O-acetyl-D-glucopyranosylidene)amino N-phenylcarbamate
CAS No.:103955-41-5
Molecular Formula:C₂₁H₂₄N₂O₁₁
Molecular Weight:480.428
Hs Code.:

Synonyms:O-(2,3,4,6-tetra-O-acetyl-D-glucopyranosylidene)amino N-phenylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(2,3,4,6-tetra-O-acetyl-D-glucopyranosylidene)amino N-phenylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of O-(2,3,4,6-tetra-O-acetyl-D-glucopyranosylidene)amino N-phenylcarbamate

There total 2 articles about O-(2,3,4,6-tetra-O-acetyl-D-glucopyranosylidene)amino N-phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 103-71-9
phenyl isocyanate

: 103955-34-6
2,3,4,6-tetra-O-acetyl-D-gluconhydroximo-1,5-lactone

: 103955-41-5
O-(2,3,4,6-tetra-O-acetyl-D-glucopyranosylidene)amino N-phenylcarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1002/hlca.19850680821

Reference yield:

: 103955-24-4
D-gluconhydroximo-1,5-lactone 1-N,2,3,4,6-pentaacetate

: 103955-41-5
O-(2,3,4,6-tetra-O-acetyl-D-glucopyranosylidene)amino N-phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / CH₃NH₂ / methanol; ethanol

2: 90 percent / Et₃N / tetrahydrofuran

With triethylamine; methylamine; In tetrahydrofuran; methanol; ethanol;
DOI:10.1002/hlca.19850680821