benzyl [(Z)-3-(1H-1,2,3-benzotriazol-1-yl)-3-(pyridin-2-ylimino)propyl]carbamate

Base Information

Chemical Name:benzyl [(Z)-3-(1H-1,2,3-benzotriazol-1-yl)-3-(pyridin-2-ylimino)propyl]carbamate
CAS No.:1374639-96-9
Molecular Formula:C₂₂H₂₀N₆O₂
Molecular Weight:400.44
Hs Code.:

Synonyms:benzyl [(Z)-3-(1H-1,2,3-benzotriazol-1-yl)-3-(pyridin-2-ylimino)propyl]carbamate

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Chemical Property of benzyl [(Z)-3-(1H-1,2,3-benzotriazol-1-yl)-3-(pyridin-2-ylimino)propyl]carbamate

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Technology Process of benzyl [(Z)-3-(1H-1,2,3-benzotriazol-1-yl)-3-(pyridin-2-ylimino)propyl]carbamate

There total 4 articles about benzyl [(Z)-3-(1H-1,2,3-benzotriazol-1-yl)-3-(pyridin-2-ylimino)propyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 71874-10-7
benzyl [3-oxo-3-(pyridin-2-ylamino)propyl]carbamate

: 1374639-96-9
benzyl [(Z)-3-(1H-1,2,3-benzotriazol-1-yl)-3-(pyridin-2-ylimino)propyl]carbamate

Guidance literature:: benzyl [3-oxo-3-(pyridin-2-ylamino)propyl]carbamate; With phosphorus pentachloride; In dichloromethane; at 40 ℃; for 2h; Inert atmosphere;

1,2,3-Benzotriazole; In dichloromethane; at 40 ℃; for 14h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.02.117

Reference yield:

: 504-29-0
2-aminopyridine

: 1374639-96-9
benzyl [(Z)-3-(1H-1,2,3-benzotriazol-1-yl)-3-(pyridin-2-ylimino)propyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.1: phosphorus pentachloride / dichloromethane / 2 h / 40 °C / Inert atmosphere

2.2: 14 h / 40 °C / Inert atmosphere

With phosphorus pentachloride; triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2012.02.117

Reference yield:

: 51513-97-4
N-[(phenylmethoxy)carbonyl]-β-alanine chloride

: 1374639-96-9
benzyl [(Z)-3-(1H-1,2,3-benzotriazol-1-yl)-3-(pyridin-2-ylimino)propyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.1: phosphorus pentachloride / dichloromethane / 2 h / 40 °C / Inert atmosphere

2.2: 14 h / 40 °C / Inert atmosphere

With phosphorus pentachloride; triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2012.02.117