N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide>

Base Information

Chemical Name:N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide>
CAS No.:101631-04-3
Molecular Formula:C₃₈H₅₄ClN₃O₃Si
Molecular Weight:664.404
Hs Code.:

Synonyms:N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide>

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Chemical Property of N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide>

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Technology Process of N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide>

There total 9 articles about N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7766-50-9
1-undecen-11-ylbromide

: 101631-04-3
N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide>

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) Na / 2.) 18-crown-6 / 1.) butanol; 2.) toluene, reflux, overnight

2: 65 percent / H₂NNH₂ / by Markees et al.

3: 9percent HCl, NaNO₂ / H₂O / 2 h / 10 - 15 °C

4: 5 h / Heating

5: 85 percent / KOH / ethanol / 3 h / Heating

6: 25 percent / N-methylmorpholine / CHCl₃ / -20 - -15 °C

7: platinic acid / 2 h / Heating

With 4-methyl-morpholine; hydrogenchloride; potassium hydroxide; sodium; hydrazine; sodium nitrite; 18-crown-6 ether; platinic acid; In ethanol; chloroform; water;
DOI:10.1021/ja00272a027

Reference yield:

: 4286-15-1
(S)-2-phenylbutyric acid

: 101631-04-3
N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide>

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / SOCl₂ / CH₂Cl₂ / 4 h / Heating

2: 25 percent / N-methylmorpholine / CHCl₃ / -20 - -15 °C

3: platinic acid / 2 h / Heating

With 4-methyl-morpholine; thionyl chloride; platinic acid; In dichloromethane; chloroform;
DOI:10.1021/ja00272a027

Reference yield:

: 40473-35-6
(S)-(+)-2-phenylbutyric acid chloride

: 101631-04-3
N,N'-<4-(11-(dimethylchlorosilyl)undecyloxy)-2,6-pyridinediyl>bis<2-(S)-phenylbutanamide>

Guidance literature:: Multi-step reaction with 2 steps

1: 25 percent / N-methylmorpholine / CHCl₃ / -20 - -15 °C

2: platinic acid / 2 h / Heating

With 4-methyl-morpholine; platinic acid; In chloroform;
DOI:10.1021/ja00272a027