[2-¹³C,4'-O¹³CH₃]4-methoxycinnamic acid

Base Information

Chemical Name:[2-¹³C,4'-O¹³CH₃]4-methoxycinnamic acid
CAS No.:1353643-95-4
Molecular Formula:C₁₀H₁₀O₃
Molecular Weight:180.166
Hs Code.:

[2-<sup>13</sup>C,4'-O<sup>13</sup>CH<sub>3</sub>]4-methoxycinnamic acid

Synonyms:[2-¹³C,4'-O¹³CH₃]4-methoxycinnamic acid

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Chemical Property of [2-¹³C,4'-O¹³CH₃]4-methoxycinnamic acid

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Technology Process of [2-¹³C,4'-O¹³CH₃]4-methoxycinnamic acid

There total 3 articles about [2-¹³C,4'-O¹³CH₃]4-methoxycinnamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 4227-95-6
[13C]methyl iodide

: 119060-98-9
[2-¹³C]4-coumaric acid

: 1353643-95-4
[2-¹³C,4'-O¹³CH₃]4-methoxycinnamic acid

Guidance literature:: With potassium carbonate; In acetone; for 4h; Reflux;
DOI:10.1016/j.phytochem.2015.07.017

Reference yield: 79.0%

: 4227-95-6
[13C]methyl iodide

: [2-¹³C]4-methoxycinnamic acid

: 1353643-95-4
[2-¹³C,4'-O¹³CH₃]4-methoxycinnamic acid

Guidance literature:: With potassium carbonate; In acetone; for 4h;
DOI:10.1016/j.phytochem.2015.05.017

Reference yield:

: [2-⁽¹³⁾C]4'-[methoxy-⁽¹³⁾C]cinnamic acid [methyl-⁽¹³⁾C] ester

: 1353643-95-4
[2-¹³C,4'-O¹³CH₃]4-methoxycinnamic acid

Guidance literature:: [2-⁽¹³⁾C]4'-[methoxy-⁽¹³⁾C]cinnamic acid [methyl-⁽¹³⁾C] ester; With water; sodium hydroxide; for 2h; Reflux;

In water; pH=Ca. 1;
DOI:10.1016/j.phytochem.2009.10.019