hexameric n-butyloxotin benzoate

Base Information

• Chemical Name: hexameric n-butyloxotin benzoate
• CAS No.: 115270-31-0
• Molecular Formula: C₆₆H₈₄O₁₈Sn₆
• Molecular Weight: 1877.64
• Mol file: 115270-31-0.mol

Synonyms:hexameric n-butyloxotin benzoate

Chemical Property of hexameric n-butyloxotin benzoate

Chemical Property:

Purity/Quality:

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Technology Process of hexameric n-butyloxotin benzoate

There total 1 articles about hexameric n-butyloxotin benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.4%

n-butylstannoic acid (2273-43-0) + benzoic acid (65-85-0,8013-63-6) → hexameric n-butyloxotin benzoate (115270-31-0)

Guidance literature:

In benzene; byproducts: water; addn. of C6H5COOH to n-butylstannoic acid in dry benzene, heating (reflux, 4 h), removal of water (azeotropic distn., Dean-Stark app.); removal of solvent (vac.), soln. of solid in hot benzene/hexane, keeping in the refrigerator; elem. anal.;

upstream raw materials:

n-butylstannoic acid

benzoic acid

Refernces

• 1、 Day, Roberta O.,Chandrasekhar,Swamy, K. C. Kumara,Holmes, Joan M.,Burton, Sarah D.,Holmes, Robert R.. "Novel drums and mixed-drum organooxotin clusters from carboxylic, phosphinic, and phosphoric acids". . p. 2887 - 2893. Retrieved 2008/10/08.