[Pd(2-thienyl)(tri(tert-butyl)phosphine)(bis(3,5-bis(trifluoromethyl)phenyl)amide)]

Base Information

Chemical Name:[Pd(2-thienyl)(tri(tert-butyl)phosphine)(bis(3,5-bis(trifluoromethyl)phenyl)amide)]
CAS No.:700378-55-8
Molecular Formula:C₃₂H₃₆F₁₂NPPdS
Molecular Weight:832.085
Hs Code.:

Synonyms:[Pd(2-thienyl)(tri(tert-butyl)phosphine)(bis(3,5-bis(trifluoromethyl)phenyl)amide)]

Suppliers and Price of [Pd(2-thienyl)(tri(tert-butyl)phosphine)(bis(3,5-bis(trifluoromethyl)phenyl)amide)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Pd(2-thienyl)(tri(tert-butyl)phosphine)(bis(3,5-bis(trifluoromethyl)phenyl)amide)]

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Technology Process of [Pd(2-thienyl)(tri(tert-butyl)phosphine)(bis(3,5-bis(trifluoromethyl)phenyl)amide)]

There total 1 articles about [Pd(2-thienyl)(tri(tert-butyl)phosphine)(bis(3,5-bis(trifluoromethyl)phenyl)amide)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1003-09-4
2-bromothiophene

: 53199-31-8
bis(tri-t-butylphosphine)palladium⁽⁰⁾

: potassium bis(3,5-bis(trifluoromethyl)phenyl)amide

: 700378-55-8
[Pd(2-thienyl)(tri(tert-butyl)phosphine)(bis(3,5-bis(trifluoromethyl)phenyl)amide)]

Guidance literature:: In neat (no solvent); 2-thienyl bromide with Pd(P(t-Bu)3)2 in the presence of potassium diarylamide;
DOI:10.1021/ja0315107

Reference yield:

: 700378-55-8
[Pd(2-thienyl)(tri(tert-butyl)phosphine)(bis(3,5-bis(trifluoromethyl)phenyl)amide)]

: 7440-05-3
palladium

Guidance literature:: With P(C(CH₃)3)3; In toluene; byproducts: (C4H3S)N(3,5-(CF3)2C6H3)2; heating in toluene to 75°C in the presence of 0-5 equiv. of phosphine; monitored by (19)F NMR spectroscopy; Kinetics;
DOI:10.1021/ja0315107