1-BUTYL-3-METHYLIMIDAZOLIUM TRICYANOMETHANIDE

Base Information

• Chemical Name: 1-BUTYL-3-METHYLIMIDAZOLIUM TRICYANOMETHANIDE
• CAS No.: 878027-73-7
• Molecular Formula: C₄N₃*C₈H₁₅N₂
• Molecular Weight: 229.285
• Mol file: 878027-73-7.mol

Synonyms:1-butyl-3-methylimidazol-3-ium tricyanomethanide

Chemical Property of 1-BUTYL-3-METHYLIMIDAZOLIUM TRICYANOMETHANIDE

Chemical Property:

• Refractive Index: 1.5070 to 1.5110

Purity/Quality:

99.3% ^*data from raw suppliers

1-Butyl-3-methylimidazolium Tricyanomethanide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-BUTYL-3-METHYLIMIDAZOLIUM TRICYANOMETHANIDE

There total 3 articles about 1-BUTYL-3-METHYLIMIDAZOLIUM TRICYANOMETHANIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

→ 1-butyl-3-methylimidazol-3-ium tricyanomethanide (878027-73-7)

Guidance literature:

Reference yield: 71.0%

sodium tricyanomethanide (36603-80-2) + 1-n-butyl-3-methylimidazolim bromide (85100-77-2) → 1-butyl-3-methylimidazol-3-ium tricyanomethanide (878027-73-7)

Guidance literature:

In water; at 20 ℃; for 20h;

DOI:10.1039/d0ob01198c

Reference yield:

sodium tricyanomethanide (36603-80-2) + 1-butyl-3-methylimidazolium chloride (79917-90-1) → 1-butyl-3-methylimidazol-3-ium tricyanomethanide (878027-73-7)

Guidance literature:

In dichloromethane; at 20 ℃; for 48h;

DOI:10.1039/c3ra45872e

upstream raw materials:

sodium tricyanomethanide

1-butyl-3-methylimidazolium chloride

1-n-butyl-3-methylimidazolim bromide

Downstream raw materials:

[BMIM]C[(CN)B(C₆F₅)3]3

Refernces

• 1、 Gilbert, Alyssa,Haines, Ronald S.,Harper, Jason B.. "Controlling the reactions of 1-bromogalactose acetate in methanol using ionic liquids as co-solvents". supporting information. p. 5442 - 5452. Retrieved 2020/09/09.