allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside

Base Information

Chemical Name:allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside
CAS No.:1351452-47-5
Molecular Formula:C₅₉H₆₈Cl₃NO₁₃Si
Molecular Weight:1133.63
Hs Code.:

allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside

Synonyms:allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside

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Chemical Property of allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside

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Technology Process of allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside

There total 2 articles about allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1351452-38-4
allyl 3-O-benzyl-6-O-tert-butyldiphenylsilyl-2-O-levulinyl-α-D-mannopyranoside

: 1351452-46-4
dibutyl 3,6-di-O-benzyl-2-deoxy-4-O-(2-naphthylmethyl)-1-seleno-2-trichloracetamido-α-D-galactopyranosyl phosphate

: 1351452-47-5
allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside

Guidance literature:: allyl 3-O-benzyl-6-O-tert-butyldiphenylsilyl-2-O-levulinyl-α-D-mannopyranoside; dibutyl 3,6-di-O-benzyl-2-deoxy-4-O-(2-naphthylmethyl)-1-seleno-2-trichloracetamido-α-D-galactopyranosyl phosphate; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 ℃; for 1h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 2.5h; pH=7.4; aq. phosphate buffer; Inert atmosphere;
DOI:10.1002/anie.201103483

Reference yield:

: C₇₀H₇₆Cl₃NO₁₃Si

: 1351452-47-5
allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In aq. phosphate buffer;
DOI:10.1039/c2sc21515b

Reference yield: 82.0%

: 74666-83-4,105990-37-2,125354-46-3,125354-47-4,125411-99-6,108739-67-9
1-deoxy-1-(S-ethyl)-2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

: 1351452-47-5
allyl 3,6-di-O-benzyl-2-deoxy-2-trichloracetamido-β-D-galactopyranosyl-(1->4)-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-levulinyl-α-D-mannopyranoside

: 1351452-48-6
C₉₃H₁₀₂Cl₃NO₁₈Si

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; N,N-dimethyl-formamide; In thiophene; toluene; at 0 ℃; for 12h; Solvent; Time; Molecular sieve; Sonication;
DOI:10.1039/c2sc21515b