C₅₇H₅₂Cl₂N₄O₈

Base Information

Chemical Name:C₅₇H₅₂Cl₂N₄O₈
CAS No.:1453486-26-4
Molecular Formula:C₅₇H₅₂Cl₂N₄O₈
Molecular Weight:991.968
Hs Code.:

C<sub>57</sub>H<sub>52</sub>Cl<sub>2</sub>N<sub>4</sub>O<sub>8</sub>

Synonyms:C₅₇H₅₂Cl₂N₄O₈

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Chemical Property of C₅₇H₅₂Cl₂N₄O₈

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Technology Process of C₅₇H₅₂Cl₂N₄O₈

There total 5 articles about C₅₇H₅₂Cl₂N₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1453486-23-1
C₅₈H₅₆Cl₂N₄O₁₀

: 1453486-26-4
C₅₇H₅₂Cl₂N₄O₈

Guidance literature:: With trifluoroacetic acid; In dimethyl sulfoxide; at 20 ℃; for 0.166667h;
DOI:10.1055/s-0033-1338868

Reference yield:

: 1453486-16-2
C₃₄H₃₀Cl₂N₂O₆

: 1453486-26-4
C₅₇H₅₂Cl₂N₄O₈

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / isopropyl alcohol / 32 h

2: sodium tetrahydroborate / tetrahydrofuran; ethanol / 8 h / 20 °C

3: trifluoroacetic acid / dimethyl sulfoxide / 0.17 h / 20 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; ethanol; dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1055/s-0033-1338868

Reference yield:

: 3,3'-bis(4-chlorophenyl)-4,4',6,6'-tetramethoxy-1H,1'H-2,7'-biindole

: 1453486-26-4
C₅₇H₅₂Cl₂N₄O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: trichlorophosphate / 8.5 h / 20 - 60 °C

1.2: 1 h / 20 °C

2.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 8 h / 20 °C

3.1: toluene-4-sulfonic acid / isopropyl alcohol / 32 h

4.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 8 h / 20 °C

5.1: trifluoroacetic acid / dimethyl sulfoxide / 0.17 h / 20 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; trifluoroacetic acid; trichlorophosphate; In tetrahydrofuran; ethanol; dimethyl sulfoxide; isopropyl alcohol; 1.1: |Vilsmeier-Haack Formylation;
DOI:10.1055/s-0033-1338868