benzyl 3--amino-3-phenyl-2-propenoate

Base Information

Chemical Name:benzyl 3--amino-3-phenyl-2-propenoate
CAS No.:170745-58-1
Molecular Formula:C₂₄H₂₃NO₂
Molecular Weight:357.452
Hs Code.:

benzyl 3-<N-(R)-1-phenylethyl>-amino-3-phenyl-2-propenoate

Synonyms:benzyl 3--amino-3-phenyl-2-propenoate

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Chemical Property of benzyl 3--amino-3-phenyl-2-propenoate

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Technology Process of benzyl 3--amino-3-phenyl-2-propenoate

There total 1 articles about benzyl 3--amino-3-phenyl-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 68199-30-4
(Z)-N-(α-Methylbenzylidene)-(R)-1-phenylethylamine

: 170745-58-1
benzyl 3--amino-3-phenyl-2-propenoate

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; for 2h; -80 deg C to rt;
DOI:10.1016/0040-4020(95)00476-O

Reference yield: 68.0%

: 170745-58-1
benzyl 3--amino-3-phenyl-2-propenoate

: benzyl (3R)-3-phenyl-3-{[(1'R)-1'-phenylethyl]amino}propanoate

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In acetonitrile; at 0 ℃; for 2h;
DOI:10.1081/SCC-100105666

Reference yield:

: 170745-58-1
benzyl 3--amino-3-phenyl-2-propenoate

: 614-19-7,3646-50-2,13921-90-9,40856-44-8
(R)-3-phenyl-3-aminopropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / NaHB(OAc)3; AcOH / acetonitrile / 2 h / 0 °C

2: 89 percent / H₂ / Pd/C / methanol / 20 °C

With hydrogen; sodium tris(acetoxy)borohydride; acetic acid; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1081/SCC-100105666