(E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol

Base Information

Chemical Name:(E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol
CAS No.:1193433-99-6
Molecular Formula:C₁₉H₂₆ClNO
Molecular Weight:319.875
Hs Code.:

Synonyms:(E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol

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Chemical Property of (E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol

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Technology Process of (E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol

There total 1 articles about (E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: C₉H₁₁O^(1-)*Li⁽¹⁺⁾

: 1032080-61-7
[1-(3-Chloro-phenyl)-meth-(E)-ylidene]-propyl-amine

: 1193433-99-6
(E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol

Guidance literature:: [1-(3-Chloro-phenyl)-meth-(E)-ylidene]-propyl-amine; With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In diethyl ether; at -78 - -40 ℃; for 2.5h; Inert atmosphere;

C₉H₁₁O^(1-)*Li⁽¹⁺⁾; In diethyl ether; at -40 - 0 ℃; for 6.5h; Inert atmosphere;

With water; sodium hydrogencarbonate; In diethyl ether; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol902169k

Reference yield: 66.0%

: 1193433-99-6
(E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol

: 75-07-0,9002-91-9
acetaldehyde

: (5R,7R,7aR,10⁽¹⁾S)-5-(3-chlorophenyl)-7-methyl-6-propyl-3,5,6,7,7a,8,9,10-octahydro-2H-cyclopenta[c]pyrano[2,3-d]pyridine

Guidance literature:: (E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol; acetaldehyde; With (1S)-10-camphorsulfonic acid; In acetonitrile; at 100 ℃; for 20h; Inert atmosphere;

With sodium hydroxide; In water; acetonitrile; at 20 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol902169k

Reference yield: 57.0%

: 110-88-3
1,3,5-Trioxan

: 1193433-99-6
(E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol

: (5S,7aR,10⁽¹⁾S)-5-(3-chlorophenyl)-6-propyl-3,5,6,7,7a,8,9,10-octahydro-2H-cyclopenta[c]pyrano[2,3-d]pyridine

Guidance literature:: 1,3,5-Trioxan; (E)-5-(3-chlorophenyl)-4-(1-cyclopentenyl)-5-(propylamino)pent-3-en-1-ol; With (1S)-10-camphorsulfonic acid; In acetonitrile; for 20h; Inert atmosphere; Reflux;

With sodium hydroxide; In water; acetonitrile; at 20 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol902169k